Propionyl chloride synthesis

NovicechemistEU

Don't buy from me
New Member
Language
🇹🇷
Joined
Nov 25, 2024
Messages
12
Reaction score
2
Points
3
Propionyl chloride, benzoyl chloride prepared via propionic acid The 1:1 molar ratio of reactants was chosen.


10 mol propionic acid ≈ 747 mL 10 mol benzoyl chloride ≈ 1161 mL (~1:1 molar ratio) in a 2000 mL flask Vertical distillation through a 200 mm column

45-69'C (most collected above 64-69'C) by evacuating a stream of HCl gas from the reaction while finally heating to 190'C to yield 340 g of distillate.
Yield 340 Gr
Note : Really very dangerous synthesis think twice. 😁
 

Attachments

  • UHobehZPwO.jpg
    UHobehZPwO.jpg
    4 MB · Views: 3
  • P801gLNbhW.jpg
    P801gLNbhW.jpg
    3.5 MB · Views: 3

NovicechemistEU

Don't buy from me
New Member
Language
🇹🇷
Joined
Nov 25, 2024
Messages
12
Reaction score
2
Points
3
Today I will try another synthesis on a large scale, 5 liters above
1/1 molar ratio 25 mol
Propionic Acid 25 mol **1869 mL
Benzoyl Chloride 25 mol **2903 mL
 
Top