- Joined
- Jun 21, 2022
- Messages
- 9
- Reaction score
- 4
- Points
- 3
Has anyone tryied shake and bake method for production of 4mmc with DCM?
Which are the risks involved?
Which are the risks involved?
Chemicals
{100g}
2-bromo-4methylopropiophenone
{500ml} dcm toulen or benzen
{200ml} methyloamine 40% in water
{3x300ml} cheap water from shop with no gas!!!
{500ml} acetone technical from the construction shop
{55ml} acid hcl 35%-38% if you have 31% acid then we need more to use
This all what we need to made this way
if I want to make a larger scale, like 1kg, I need to multipliate by 10 the reagents ect..?
Chemicals
{100g}
2-bromo-4methylopropiophenone
{500ml} dcm toulen or benzen
{200ml} methyloamine 40% in water
{3x300ml} cheap water from shop with no gas!!!
{500ml} acetone technical from the construction shop
{55ml} acid hcl 35%-38% if you have 31% acid then we need more to use
This all what we need to made this way
U said "cheap water from shop" but u dont need to use distillate water? Demineralized water can be good?
to completely seal the jar. When I pour methylamine, the gas cannot escape, then in addition I seal the jar with the tape.
Why the bag? Can you explain more please
You get 4mmc freebase in dcm on top you have monomethyloamine
You take out monomethyloamine and drop water and wash later we have
4mmc freebase oil
Video shake and bake
whats the yield? Not a lot I imagine..?
Our team brings together the best specialists from different fields.
We are ready to share our experience, discuss difficult issues and find new solutions.
Connect notifications to always stay in touch with the forum!
The BB Forum team is looking for cooperation: