- Joined
- Mar 12, 2023
- Messages
- 80
- Reaction score
- 34
- Points
- 18
Could you tell what laboratory equipment is required for the chemical synthesis of 2-CB?
- By w2x3f5
Could you tell what laboratory equipment is required for the chemical synthesis of 2-CB?
↑View previous replies…
w2x3f5i want to follow the chemical syntesis of 2-CB posted in this post
chemistry.mobHenry reaction, flask, reflux condenser, heated magnetic stirrer, water bath (or do it in the microwave), measuring cylinder, vacuum filter Buchner funnel and Bünsen flask and the filters themselves, heat-resistant beakers low spout
Reduction on lithium aluminum hydride is all the same, only ice and a dropping funnel will be needed to drop the styrene solution, and then we drop in ethyl acetate or ethyl alcohol in order to use up the excess lithium aluminum hydride.
Bromination is the same
scales and the like.
chemistry.moblithium aluminum hydride doesn't like jokes and likes to explode and set fire to solvents. it cannot be extinguished with water, carbon dioxide, else he not like peroxide and water in THF
w2x3f5So it would be better to use a chemical reactor to prevent it from exploding and harming me? And if so, what capacity should the chemical reactor be?
Have you made 2C-B before?
thanks!
chemistry.mobhow will the reactor help you? work correctly with lithium aluminum hydride, everything is as dry as possible, good cooling, the absence of peroxide impurities in the solvent.
I did it in an ordinary three-necked flask in an ice bath, sometimes with explosions and fires, in the first syntheses, then I learned =)
chemistry.mobIt would be better to just not use THF if youre asking questions like this
UWe9o12jkied91dbad advice) I can already imagine how dry styrene is mixed with aluminum hydride (dioxane has the same problems of fluorine and thf)
UWe9o12jkied91dmate, I have no idea about chemistry, I'm trying to learn, but it's frustrating, too much information, I still don't know which chemical synthesis to stay with and focus on it, I'm thinking either 2-CB or MDMA, unless I changed my mind, at first I wanted to do the synthesis of LSD but I have seen that the synthesis for the manufacture of only lysergic acid, the precursor of LSD, is very complex and requires many reagents and chemical reactions.
thank you!
chemistry.mobLAH not for beginner
w2x3f5My friend, from where did you bought (CAS: 93-02-7)?
And what´s the difference between that and this 2,5-dimethoxy-beta-nitrostyrene?
Thank you! and sorry, but i have no idea about chemistry.
chemistry.mobthe first is aldehyde, the second is nitrostyrene. the difference besides the fact that in the formula, they have different physical and chemical properties
check melting point
chemistry.mobI have both the styrene and aldehyde for sale if you are interested.
UWe9o12jkied91dWhat´s the price?
chemistry.mob180 euros for 100g of the styrene and 120 euros for 100g of the aldehyde
UWe9o12jkied91dThe problem is that I don't know that with 100g how much 2-CB I can get
chemistry.mobSound like a you problem
chemistry.mobAgain, sounds like a you problem
- Joined
- Mar 12, 2023
- Messages
- 80
- Reaction score
- 34
- Points
- 18
it all depends on the way of synthesis. you need a starting point and the path you want to follow.
i want to follow the chemical syntesis of 2-CB posted in this post
Reduction on lithium aluminum hydride is all the same, only ice and a dropping funnel will be needed to drop the styrene solution, and then we drop in ethyl acetate or ethyl alcohol in order to use up the excess lithium aluminum hydride.
Bromination is the same
scales and the like.
i want to follow the chemical syntesis of 2-CB posted in this post
- Joined
- Mar 12, 2023
- Messages
- 80
- Reaction score
- 34
- Points
- 18
lithium aluminum hydride doesn't like jokes and likes to explode and set fire to solvents. it cannot be extinguished with water, carbon dioxide, else he not like peroxide and water in THF
Have you made 2C-B before?
thanks!
So it would be better to use a chemical reactor to prevent it from exploding and harming me? And if so, what capacity should the chemical reactor be?
Have you made 2C-B before?
thanks!
I did it in an ordinary three-necked flask in an ice bath, sometimes with explosions and fires, in the first syntheses, then I learned =)
- Joined
- Aug 8, 2022
- Messages
- 679
- Reaction score
- 501
- Points
- 63
- Deals
- 5
So it would be better to use a chemical reactor to prevent it from exploding and harming me? And if so, what capacity should the chemical reactor be?
Have you made 2C-B before?
thanks!
It would be better to just not use THF if youre asking questions like this
- Joined
- Mar 12, 2023
- Messages
- 80
- Reaction score
- 34
- Points
- 18
It would be better to just not use THF if youre asking questions like this
thank you!
mate, I have no idea about chemistry, I'm trying to learn, but it's frustrating, too much information, I still don't know which chemical synthesis to stay with and focus on it, I'm thinking either 2-CB or MDMA, unless I changed my mind, at first I wanted to do the synthesis of LSD but I have seen that the synthesis for the manufacture of only lysergic acid, the precursor of LSD, is very complex and requires many reagents and chemical reactions.
thank you!
- Joined
- Mar 12, 2023
- Messages
- 80
- Reaction score
- 34
- Points
- 18
how will the reactor help you? work correctly with lithium aluminum hydride, everything is as dry as possible, good cooling, the absence of peroxide impurities in the solvent.
I did it in an ordinary three-necked flask in an ice bath, sometimes with explosions and fires, in the first syntheses, then I learned =)
2,5-Dimethoxybenzaldehyde
I found a seller on alibaba that supposedly sells it, but how can I make sure that is that substance when I receive it?And what´s the difference between that and this 2,5-dimethoxy-beta-nitrostyrene?
Thank you! and sorry, but i have no idea about chemistry.
My friend, from where did you bought (CAS: 93-02-7)?
2,5-Dimethoxybenzaldehyde
I found a seller on alibaba that supposedly sells it, but how can I make sure that is that substance when I receive it?
And what´s the difference between that and this 2,5-dimethoxy-beta-nitrostyrene?
Thank you! and sorry, but i have no idea about chemistry.
check melting point
- Joined
- Aug 8, 2022
- Messages
- 679
- Reaction score
- 501
- Points
- 63
- Deals
- 5
My friend, from where did you bought (CAS: 93-02-7)?
2,5-Dimethoxybenzaldehyde
I found a seller on alibaba that supposedly sells it, but how can I make sure that is that substance when I receive it?
And what´s the difference between that and this 2,5-dimethoxy-beta-nitrostyrene?
Thank you! and sorry, but i have no idea about chemistry.
- Joined
- Mar 12, 2023
- Messages
- 80
- Reaction score
- 34
- Points
- 18
I have both the styrene and aldehyde for sale if you are interested.
- Joined
- Aug 8, 2022
- Messages
- 679
- Reaction score
- 501
- Points
- 63
- Deals
- 5
What´s the price?
- Joined
- Mar 12, 2023
- Messages
- 80
- Reaction score
- 34
- Points
- 18
180 euros for 100g of the styrene and 120 euros for 100g of the aldehyde
- Joined
- Aug 8, 2022
- Messages
- 679
- Reaction score
- 501
- Points
- 63
- Deals
- 5
The problem is that I don't know that with 100g how much 2-CB I can get
- Joined
- Mar 12, 2023
- Messages
- 80
- Reaction score
- 34
- Points
- 18
- Joined
- Aug 8, 2022
- Messages
- 679
- Reaction score
- 501
- Points
- 63
- Deals
- 5
I already told you, that i have no idea about chemistry.