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Synthesis of Benzyl Cyanide from Benzyl Chloride

William D.

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Reaction scheme:
ErSgjAd5Jc



Synthesis:
1. The reactor alternately load 215 liters of purified water, 126 kg of acetone, 4 kg of triethylamine, 6 kg of potassium iodide, 165 kg of sodium cyanide and 1500 litres of 30% trichloroethylene solution of benzyl chloride.
2. The reaction mass is heated to a temperature of 85 *C, and then stirred for 6 hours.
3. Next the reactor was added purified water in an amount of 500 liters.
4. The reaction mass is heated to a temperature of 60 *C, stirred, then defended for 4 hours at the same temperature.
5. The bottom layer is transferred to the reactor, heats up to a temperature of 80 *С and trichloroethylene is distilled off (~1000 liters).
 
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KGB69

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Can I use potassium cyanide instead?
Trichloroethylene has been distilled (1000 liters).
Do I need to distill more benzyl cyanide?

William Dampier

 

G.Patton

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