1-Phenyl-2-nitropropen (P2NP) Video Synthesis From Benzaldehyde and Nitroethane. Henry-reaktion.

HIGGS BOSSON

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Problemerne med nitroethan i Europa begyndte tilbage i 2007, og efterhånden indførte alle lande restriktioner for dette værdifulde reagens. Og nu er der to måder: at lede efter leverandører i lande, hvor der er svag lovgivning med en udviklet kemisk industri, for eksempel Bangladesh, eller at syntetisere uafhængigt, hvilket vi har foreslået en metode til.
 

Alojz

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Hvad kan bruges til at erstatte eller syntetisere nitroethan?
 

Kvadprime

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You can find methods of syntes nitroethane in another thread
 

Kvadprime

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I have aniline as a base - what yeilds can it give?
 

G.Patton

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Try and figure out. Share us your research data. In theory, it's quite weak base and it would be not enough to eliminate -OH group.
 

Kvadprime

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ok, I'll definitely write how everything went... I'm still waiting for my new labware to arrive

Thx
 

rampage

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has anyone done the microwave version of this synthesis, curious as to the outcome?
 
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