PMK-oliesyntese fra PMK (CAS 28578-16-7 voksform) i stor skala

[Curiousonion]

Denne metode er for pmk CAS 28578-16. Så du kan få det i pulverform, og så bliver det til olie, når du er færdig med reaktionen.
Men det virker ekstremt nemt, er der nogen, der har prøvet det?

 

[C14]

It is bullshit from powder pmk dont work

 

[G.Patton]

This post is a good explanation, which was posted @btcboss2022 (thank you). I confirm, that it is a proven and working method.

 

[C14]

Hello the pmk powder gkyciate got one special smell?? Maybe i.got fake pmk

 

[ukises]

Hello Funciona.para el pmk ethyl powder???

 

[C14]

Your methode Dont work for pmk powder

 

[G.Patton]

Hello, the method in this topic work for PMK methyl glycidate as well

 

[C14]

Methyl , but really for pmk ethyl powder dont work,thanks

 

[Jordan Belfort]

You mean that dark pmk powder with only desolved with ethanol/alcohol @C14

 

[G.Patton]

Are you sure that you have PMK ethyl glycidate?

 

[C14]

Really now not sure, i am cheking my pmk powder dont have any smell , i mean odor, it is neutro

 

[G.Patton]

It's not a test, check its melting point and compare with a literature data.

 

[C14]

If is oil pmk, how i can know if is original or not?

 

[G.Patton]

I'm talking about its precursor PMK methyl glycidate. P2P can be checked by its boiling point, density.

 

[C14]

Hello meting point is 66 degrees c ?. Dificul find this information, thanks

 

[btcboss2022]

HVIS
Hvis du fulgte processen trin for trin, skulle du have 2 lag, forklar mig punkt for punkt, hvad du præcist gør

 

[C14]

Hello i got pmk.glicidate i dont know exactly cas number, but is white not shinning , it is fatty , In water in ph 10, i cooked 2 times with naoh and hcl but after i use hcl start precipitatie white powder again, i think that is not.necesary use naoh becouse the ph is alcal ine, you got any idea?

 

[Win Win]

Hej, kan jeg bruge denne metode?
1. Tilsæt 100 ml ethanol til 100 g PMK-pulver, og tilsæt derefter 100 ml destilleret vand, og forsegl og omrør ved stuetemperatur i 90 minutter, indtil det bliver lidt pulveragtigt.
2. Filtrer væsken (vej pulveret), og tilsæt saltsyre i forholdet 1:2.
3. Hæld pulveret i reaktionskedlen, tilsæt saltsyre, begynd at røre, hæv temperaturen til 75 grader, og rør i 3 timer. Du vil se et mørkt, olieagtigt stof.
4. Tag olien ud og brug den til næste trin.

 

[C14]

Hello for 100 grms pmk, how many grams of hcl? Thanks

 

[C14]

Hello Hcl radio 1:2 you mean 100 gr pmk and 200 gram hcl?

 

[realboss]

. Add 3.25kg of HCL 37% in small portions, once all added keep the mixture at 80 °C reflux during 1 h stirring.
hcl 37% water solution ?

 

[C14]

Hello for what use.the s bicarbonate, for clean or.for change ph?

 

[Jordan Belfort]

Both, and probably some NaCl will be formed if aquous HCL has been used, resulting in general better kinetics (if minor trace stays in the oil).

 

[G.Patton]

It's need to carry out alkaline hydrolysis of ester.

 

[C14]

Hello , this one Add 3.25kg of HCL 37% pure. Not with something water? Thanks