Synthese von 5-MeO-DMT aus 5-MeO-Tryptamin

MadHatter

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Hamilton Morris tut dies auf Youtube:
Das Labor, in dem er arbeitet, ist ein echter Laborporno. Dient zur Veranschaulichung dieses ausgezeichneten Textes!
 

mycelium

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Danke, Hutmacher
 

tripeep

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Wie viele Milliliter einer 37%igen Formaldehydlösung werden benötigt?
 
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G.Patton

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Bitte verwenden Sie in den allgemeinen Abschnitten die englische Sprache.
 
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tripeep

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Wie viele ml einer 37%igen Formaldehydlösung werden benötigt?
 

G.Patton

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Hallo, äquimolare Menge 26,25 mmol (als 5-MeO-Tryptamin). Zählen Sie es in 37%iger wässriger Lösung.
 

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Kann Natriumborhydrid durch Kaliumborhydrid mit der gleichen Anzahl von mmol ersetzt werden?
 

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It says a solution of 37% formaldehyde stabilized w 12% meoh , which I assume to be an 88% formalin and 12% meoh, an I correct? Or would it be 100% formalin and 12% MeOH?
 

bigdigrandy

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Würde eine Reduktion mit Natriumhydrid auch funktionieren, weil NaBH4 dort, wo ich wohne, reguliert ist, aber ich habe einen vertrauenswürdigen Anbieter für NaH gefunden
 

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Kann Natriumborhydrid durch Kaliumborhydrid mit der gleichen Anzahl von mmol ersetzt werden?
 

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mycelium

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Wow, that is amazing.
I have lots of experience with dry ice baths, and lots of experience with throwing scoops of DI into the alcohol in the condenser , and it just exploding into the lab...dry ice and IPA.. ALCOHOL(OR ACETONE) into the dry ice works a lot better.
And hearing the stainless squeak and sound like it is ripping apart, just from the temp change ..
 
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