Synteesi 5-MeO-DMT:stä 5-MeO-tryptamiinista

MadHatter

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Hamilton Morris tekee tätä Youtubessa:
Laboratorio, jossa hän työskentelee, on todellista laboratoriopornoa. Toimii tämän erinomaisen kirjoituksen kuvituksena!
 

mycelium

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Thanks, hatter
 

tripeep

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Kuinka monta millilitraa 37-prosenttista formaldehydiliuosta tarvitaan?
 
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G.Patton

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Pyydämme käyttämään englannin kieltä yleisissä osioissa.
 
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tripeep

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Kuinka monta ml 37-prosenttista formaldehydiliuosta tarvitaan?
 

G.Patton

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Hei, ekvimolaarinen määrä 26,25 mmol (5-MeO-tryptamiinina). Laske se 37 %:n aq-liuokseen.
 

tripeep

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Voidaanko natriumboorihydridi korvata kaliumboorihydridillä samalla mmol-määrällä?
 

mycelium

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It says a solution of 37% formaldehyde stabilized w 12% meoh , which I assume to be an 88% formalin and 12% meoh, an I correct? Or would it be 100% formalin and 12% MeOH?
 

bigdigrandy

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Toimisiko pelkistäminen natriumhydridillä myös, koska NaBH4 on säännelty siellä, missä asun, mutta olen löytänyt luotettavan myyjän NaH:lle.
 

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Voidaanko natriumboorihydridi korvata kaliumboorihydridillä samalla mmol-määrällä?
 

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mycelium

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Wow, that is amazing.
I have lots of experience with dry ice baths, and lots of experience with throwing scoops of DI into the alcohol in the condenser , and it just exploding into the lab...dry ice and IPA.. ALCOHOL(OR ACETONE) into the dry ice works a lot better.
And hearing the stainless squeak and sound like it is ripping apart, just from the temp change ..
 
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