Metamfetamin efedrinből jód és vörös P segítségével

hacke8

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Elnézést, többször is elküldtem.
 

TheNut22

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Használhatok csak KI kristályokat, kivéve azokat a jodon kristályokat ebben a szintézisben, tudja? Ki tudom vonni a jódot abból a KI-ből, de amit olvastam ...
 

Anarchy Labz

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Miért használt dcm-t, lehet ezt dcm nélkül is megcsinálni? Szintén nem túlzás 12 g I2-t használni 6 g efedrinhez?
 

GhostChemist

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Használhatja a petróleumétert, a benzolt vagy a toluolt
 

Bmth

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Melyik a jobb a matrózok közül i Melyik a jobb az ilyen típusú matrózok közül az én országomban nehéz találni
Indonéziai:
 

TheNut22

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Használhatok xilolt a DCM helyett?
 

handle

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Melyik szakaszban keletkezne foszgén?
 

hacke8

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Nem fog foszgént előállítani. Foszfhidrogéngáz lesz, ha 130-nál több lesz. Legyen óvatos ezzel.
 
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TheNut22

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Igen! :). Amikor ezt a szintézist végzem, ha PVC-tömlőt teszek a kondenzátorból egy nátrium-karbonáttal és aktív szénnel teli gázcsapdába, mit tehetek, hogy megakadályozzam, hogy a gázcsapda vízoldata visszaszívja a reakciós üvegembe? Adtál ötleteket, Kézfogantyú?
 

rampage

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use a condom ontop of condenser
 

bigclit

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Tud valaki linkelni nekem egy olyan egyfazékos módszert, ahol minden anyagot személyesen kaphatok. Idc ha csak a végén néhány piszkos met csak keres egy projektet, míg a feleség a városon kívül van a hétvégén.
 

Hypnou

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Duuuude kérem, ne tegye, tényleg létezik sok jobb módszer, amit megtaníthat magának, csak a főzés tiszteletére 🫠.
 

iceberg

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Hány ml legyen az üvegballon, és milyen legyen a reflux kondenzátor? Tudna válaszolni, kérem?
 

G.Patton

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Milyen léggömbről van szó? Standard Allihn reflux kondenzátor, közepes méretű.
 

iceberg

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A listában szerepel az NH4Cl és a H2SO4. Pontosan hol használják ezeket a szintézisben? Köszönöm a választ.
 

micked24

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Ammonium Chloride and Sulfuric Acid are combined to produce Hydrogen Chloride. Which is a gas that is used to turn the freebase into a hydrochloride salt. It is used towards the end of the video.
 

TheNut22

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Használhatok xilolt a DCM helyett?
 

TheNut22

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Nos, azt hiszem, ez sikerül.
 

GhostChemist

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if o-xylene this is bad idea (B.P. 144C)
better petroleum ether, diethyl ether, benzene, toluene etc.
 

Pinkbay

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Ha szabad bázis készítésekor vizet és hcl-t adok a szabad bázis savasításához, leválasztom a vízréteget, és a vizet teljesen elpárologtatom, akkor a végén só jelenik meg? Elméletileg hidrogén-kloridra nincs szükség?
 

GhostChemist

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When the free base extracted with DCM, you can use aqueous HCl for obtain salt after evaporation
 

rampage

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can phenylpropanolamine be used instead of ephedrine in this synth?
 

William D.

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Yes. If you have a supplier, send me a DM. The only problem is that the yield may be less than with the methylated version.
 

Chemtrail

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Seen that chemical on an Asian (India) chemical company for good price

Think that chemical is being used as an animal dog medicine
 

Chemtrail

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Swim had done this "red, white, blue" process with 6g E, 6g I, 3 g Rp and a couple of mls of D-H20 in a heat proof Corona beer glass bottle as a RXN vessel, a rubber stopper with airleak-proof connection with 5 foot tubing vertical and a punch balloon as a condenser, used a portable rice cooker & sand bath as heat source ~100-120C for 24 hours

Long Wet Reaction

Off heat to cool. Add 100 ml D-H20 . Filter Rp (**WASH OUT THE RP WITH HOT ACID, HOT ALCOHOL, HOT ACETONE, lukewarm water** good as new)
Add NaOH base solution till pH 12 A WHITE SLURRY WILL APPEAR
Extract with a NP fuel several times
Wash NP fuel/chilli with baking soda solution and then a D-H20 wash
Dry with drying agent for minutes and filter

Get a shot glass of D-H20 and drop 2-3 drops of HCl (or sulfuric acid) in it. Put this shot glass water with the NP/chilli and shake

Repeat several times

Extract water/chilli and evaporate on LOW heat

Speed a few hundred milligrams but good



* Swim got a VERY small percent yeild doing this method :(

Why did swim with 6 G of pseudoephedrine ended up with just a few hundred milligrams of speed ?! :(
 

Chemdog010297

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Can we get a synthesis of two for propiophenone ?
 

Chemtrail

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Think you can make synthetic Ephedrine from propiophenone, there is a video

And don't seem very complicated
 

Chemdog010297

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Can I do this synthesis at 140 Fahrenheit for 48 hours and get the same result ?
 
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