3-Chloromethcathinone (3-CMC) Synthesis

[Abus]

From freebase 3cmc made crystal this is How to looks like.
Product what use
2b3chl
Methyloamine hcl and naoh and water
Baking soda
Water
Acid+water
IPA
In future will be use 2i3chl because in Europa will be banned in this year 2025r 2b3chl

 

[Torreto]

How long You wait for finally results?

 

[SunDay]

Good evening.
I want to try this method, becouse evaporation of aqua layer tooks too much time for me, but with DCM. do 3cmc hcl in watter not getting to ice when put in freezer?

 

[G.Patton]

Hello, your request is unclear. Please, reformulate it correctly.

 

[Dr. MMX]

within 12h alcohol + h2o solution in such proportions will be a little like just a gel, or even still liquid. It can be put out in the "correct moment " in case it will be more "like ice" if -18 c is used

If DCM is used for the synthesis, the product can be extracted with H2O after acidification.
I dont know the details, but I think its more optimal to evaporate it under pressure if we have just h2o, rather than putting it before its freezing point, I think it will be still needed to be evaporated.

 

[SunDay]

And again, you the best! I dont know how what is the pressure, but used vacuum, like you advised me before!!! Now it goes fast and well!!!

 

[SunDay]

And one more thought. If i put acetone in solution, maybe its not freezin -10, and result will be much better?

 

[Torreto]

How long You wait for finally results?