MDMA/ecstasy zuiveringsmethode

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Hallo vrienden, bedankt voor de bijdrage, het werkt heel goed maar ik heb een twijfel, bij het kristalliseren (kristallen slaan heel goed neer) krijg ik geen kristallen zoals de typische kristallen van mdma, het lijkt meer op sneeuwvlokken, op ijsvorst in een glas op een besneeuwde dag, het is glas maar heel breekbaar. Waarom krijg ik geen sterk glas? Dank u en groeten 😊
 

G.Patton

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Hallo, graag gedaan! Gebruik je een koelkast voor de kristallisatieprocedure? Hoe sneller de afkoeling, hoe kleiner de kristallen.
 
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Ja, natuurlijk, eerst laat ik het eruit tot het op kamertemperatuur is, dan is 15 of 20% al gekristalliseerd, dan zet ik het 2 uur in de koelkast en dan 3 uur in de vriezer. Bijna 100% van het gewassen product kristalliseert, maar de kristallen zijn erg breekbaar, wanneer ze worden behandeld voor verpakking veranderen ze in zand.
 

Mr Good Cat

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Ik heb IPA een paar keer gedaan en ik denk dat deze "zand" kristalstijl een natuurlijke eigenschap is van IPA kristallisatie. Probeer het te herkristalliseren in water om grote bergkristallen te krijgen.
 
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Mr Good Cat

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Wat ik heb gemerkt, is dat IPA goed is om kleverige zwarte verbinding, bijproduct van synthese, te verwijderen.
 

William Dampier

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Large crystals are obtained with the inclusion of a water molecule. Therefore, sometimes it is better to use aq. HCl acid or add water additionally. You must begin crystallization at room temperature so that the process does not begin quickly. If you show a photo of your crystals, maybe I will tell you that you can change for this and get it in a larger size.
 

Keychainsaw

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I read heat makes it brown in here,
I had some issues with the hobby project. The sirup smelled like methylamine in the glass tray and im afraid there might be some methylamine hcl in the end product. Either way this looks fucked up and it looks like it doesnt want to dry any further. Acetone wash just usually turns it into a black tar. Have to say i forgot to dry it does the 4% aq make a bid difference?

This is what i managed to scrape together and kind of dry out. It tastes more salty than bitter. I dont know how methylamine hcl tastes but drying in the oven doesn't make it appear dryer. Its more tarlike than anything else. I'm ready to give up and just flush it. I did manage to get a whiter one with acetone wash but it has the same non bitter taste. Slightly salty. Could other salts have formed in the process? Maybe the aq layer was pipetted up aswell, in that case it might contain trace amounts of mercury?
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G.Patton

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Have you dried this in an oven? At what temp? I assume, there are not a lot of MDMA in this "product".
Looks looks dog shit.
 

Keychainsaw

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105 Celcius. I did manage to get a few gr of good stuff out it before with acetone washes it yielded only a few gr. Thanks for confirming to toss it than i stop wasting and experimenting on it. To be honest the taste test did not pass and it tasted salty and slightly metallic. It didnt want to dry or crash i will simply dump it. Thanks for the fast reply.
 
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