Methamfetamine uit efedrine door jodium en rode P

hacke8

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Sorry, ik heb het meerdere keren verstuurd.
 

TheNut22

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Kan ik alleen KI-kristallen behalve die jodon-kristallen gebruiken in deze synthese? Ik kan jodium uit die KI halen, maar wat ik gelezen heb ...
 

Anarchy Labz

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Waarom heb je dcm gebruikt, kan dit ook zonder dcm? Is het niet een beetje veel om 12 g I2 te gebruiken voor 6 g efedrine?
 

GhostChemist

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Je kunt petroleumether, benzeen of tolueen gebruiken
 

Bmth

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Welke is de betere van alle matrozen i Welke van deze soorten matrozen is beter in mijn land is moeilijk te vinden
Indonesisch:
 

TheNut22

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Kan ik xyleen gebruiken in plaats van DCM?
 

handle

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In welk stadium zou er fosgeen gegenereerd worden?
 

hacke8

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Het zal geen fosgeen produceren. Er zal fosforwaterstofgas ontstaan als het meer dan 130 is. Wees hier voorzichtig mee.
 
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TheNut22

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Yep! :). Als ik deze synthese doe, als ik een PVC-slang van de condensor naar een gasvanger vol natriumcarbonaat en actieve kool leg, wat kan ik dan doen om te voorkomen dat de wateroplossing uit de gasvanger terugzuigt naar mijn reactiefles? Heeft u ideeën, handgreep?
 

rampage

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use a condom ontop of condenser
 

bigclit

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Kan iemand mij een link geven naar een one pot-methode waarbij ik alle materialen persoonlijk kan krijgen? Het maakt me niet uit of ik met wat vieze meth eindig, ik ben gewoon op zoek naar een project terwijl mijn vrouw een weekend de stad uit is.
 

Hypnou

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Doe het alsjeblieft niet, er bestaan echt veel betere methodes die je jezelf kunt aanleren, alleen al voor het respect voor koken 🫠
 

iceberg

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Hoeveel ml moet de glazen ballon zijn en hoe moet de refluxkoeler zijn? Kunt u alstublieft antwoorden?
 

G.Patton

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Over welke ballon heb je het? Standaard Allihn reflux condensor, gemiddelde grootte.
 

iceberg

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Er staat NH4Cl en H2SO4 in de lijst. Waar worden deze precies gebruikt in synthese? Bedankt voor het antwoord.
 

micked24

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Ammonium Chloride and Sulfuric Acid are combined to produce Hydrogen Chloride. Which is a gas that is used to turn the freebase into a hydrochloride salt. It is used towards the end of the video.
 

TheNut22

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Kan ik xyleen gebruiken in plaats van DCM?
 

TheNut22

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Nou, ik denk dat ik dat kan.
 

GhostChemist

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if o-xylene this is bad idea (B.P. 144C)
better petroleum ether, diethyl ether, benzene, toluene etc.
 

Pinkbay

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Als ik bij het maken van een vrije base water en hcl toevoeg om de vrije base aan te zuren, de waterlaag scheid en het water volledig verdamp, zal er dan uiteindelijk zout verschijnen? Is waterstofchloride in theorie niet nodig?
 

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When the free base extracted with DCM, you can use aqueous HCl for obtain salt after evaporation
 

rampage

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can phenylpropanolamine be used instead of ephedrine in this synth?
 

William D.

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Yes. If you have a supplier, send me a DM. The only problem is that the yield may be less than with the methylated version.
 

Chemtrail

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Seen that chemical on an Asian (India) chemical company for good price

Think that chemical is being used as an animal dog medicine
 

Chemtrail

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Swim had done this "red, white, blue" process with 6g E, 6g I, 3 g Rp and a couple of mls of D-H20 in a heat proof Corona beer glass bottle as a RXN vessel, a rubber stopper with airleak-proof connection with 5 foot tubing vertical and a punch balloon as a condenser, used a portable rice cooker & sand bath as heat source ~100-120C for 24 hours

Long Wet Reaction

Off heat to cool. Add 100 ml D-H20 . Filter Rp (**WASH OUT THE RP WITH HOT ACID, HOT ALCOHOL, HOT ACETONE, lukewarm water** good as new)
Add NaOH base solution till pH 12 A WHITE SLURRY WILL APPEAR
Extract with a NP fuel several times
Wash NP fuel/chilli with baking soda solution and then a D-H20 wash
Dry with drying agent for minutes and filter

Get a shot glass of D-H20 and drop 2-3 drops of HCl (or sulfuric acid) in it. Put this shot glass water with the NP/chilli and shake

Repeat several times

Extract water/chilli and evaporate on LOW heat

Speed a few hundred milligrams but good



* Swim got a VERY small percent yeild doing this method :(

Why did swim with 6 G of pseudoephedrine ended up with just a few hundred milligrams of speed ?! :(
 

Chemdog010297

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Can we get a synthesis of two for propiophenone ?
 

Chemtrail

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Think you can make synthetic Ephedrine from propiophenone, there is a video

And don't seem very complicated
 

Chemdog010297

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Can I do this synthesis at 140 Fahrenheit for 48 hours and get the same result ?
 
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