Metamfetamina z efedryny za pomocą jodu i czerwieni P

hacke8

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Przepraszam, wysłałem to wielokrotnie.
 

TheNut22

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Czy w tej syntezie mogę użyć samych kryształów KI oprócz kryształów jodonu? Mogę wyekstrahować jod z tego KI, ale z tego co czytałem ...
 

Anarchy Labz

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Dlaczego użyłeś dcm, czy można to zrobić bez dcm? Czy użycie 12 g I2 na 6 g efedryny to nie za dużo?
 

GhostChemist

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Możesz użyć eteru naftowego, benzenu lub toluenu
 

Bmth

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Który z tych typów żeglarzy jest lepszy w moim kraju jest trudny do znalezienia.
Indonezyjski:
 

TheNut22

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Czy mogę użyć ksylenu zamiast DCM?
 

handle

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Na jakim etapie zostanie wygenerowany fosgen?
 

hacke8

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Nie będzie produkować fosgenu. Jeśli jego stężenie przekroczy 130, powstanie fosforowodór. Należy zachować ostrożność.
 
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TheNut22

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Tak! :). Kiedy przeprowadzam tę syntezę, jeśli podłączę wąż PVC ze skraplacza do pułapki gazowej pełnej węglanu sodu i węgla aktywnego, co mogę zrobić, aby zapobiec zasysaniu roztworu wodnego pułapki gazowej z powrotem do mojej butelki reakcyjnej? Masz jakieś pomysły?
 

rampage

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use a condom ontop of condenser
 

bigclit

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Czy ktoś może mi podać link do metody jednogarnkowej, w której mogę osobiście uzyskać wszystkie materiały. Idc, jeśli skończę tylko z brudną metą, szukając projektu, podczas gdy żona jest poza miastem na weekend.
 

Hypnou

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Duuuude, proszę, nie rób tego, naprawdę istnieje wiele lepszych metod, których możesz się nauczyć, tylko dla szacunku do gotowania 🫠
 

iceberg

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Ile ml powinien mieć szklany balon, a ile chłodnica zwrotna? Proszę o odpowiedź.
 

G.Patton

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O jakim balonie mówisz? Standardowy chłodnica zwrotna Allihn, średniej wielkości.
 

iceberg

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Na liście znajdują się NH4Cl i H2SO4. Gdzie dokładnie są one używane w syntezie? Dziękuję za odpowiedź.
 

micked24

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Ammonium Chloride and Sulfuric Acid are combined to produce Hydrogen Chloride. Which is a gas that is used to turn the freebase into a hydrochloride salt. It is used towards the end of the video.
 

TheNut22

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Czy mogę użyć ksylenu zamiast DCM?
 

TheNut22

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Cóż, myślę, że mogę.
 

GhostChemist

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if o-xylene this is bad idea (B.P. 144C)
better petroleum ether, diethyl ether, benzene, toluene etc.
 

Pinkbay

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Jeśli dodam wodę i chlorowodór w celu zakwaszenia wolnej zasady podczas tworzenia wolnej zasady, oddzielę warstwę wody i całkowicie odparuję wodę, czy na końcu pojawi się sól? Teoretycznie chlorek wodoru nie jest potrzebny?
 

GhostChemist

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Gdy wolna zasada jest ekstrahowana za pomocą DCM, można użyć wodnego HCl do uzyskania soli po odparowaniu
 

rampage

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can phenylpropanolamine be used instead of ephedrine in this synth?
 

William D.

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Yes. If you have a supplier, send me a DM. The only problem is that the yield may be less than with the methylated version.
 

Chemtrail

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Seen that chemical on an Asian (India) chemical company for good price

Think that chemical is being used as an animal dog medicine
 

Chemtrail

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Swim had done this "red, white, blue" process with 6g E, 6g I, 3 g Rp and a couple of mls of D-H20 in a heat proof Corona beer glass bottle as a RXN vessel, a rubber stopper with airleak-proof connection with 5 foot tubing vertical and a punch balloon as a condenser, used a portable rice cooker & sand bath as heat source ~100-120C for 24 hours

Long Wet Reaction

Off heat to cool. Add 100 ml D-H20 . Filter Rp (**WASH OUT THE RP WITH HOT ACID, HOT ALCOHOL, HOT ACETONE, lukewarm water** good as new)
Add NaOH base solution till pH 12 A WHITE SLURRY WILL APPEAR
Extract with a NP fuel several times
Wash NP fuel/chilli with baking soda solution and then a D-H20 wash
Dry with drying agent for minutes and filter

Get a shot glass of D-H20 and drop 2-3 drops of HCl (or sulfuric acid) in it. Put this shot glass water with the NP/chilli and shake

Repeat several times

Extract water/chilli and evaporate on LOW heat

Speed a few hundred milligrams but good



* Swim got a VERY small percent yeild doing this method :(

Why did swim with 6 G of pseudoephedrine ended up with just a few hundred milligrams of speed ?! :(
 

Chemdog010297

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Can we get a synthesis of two for propiophenone ?
 

Chemtrail

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Think you can make synthetic Ephedrine from propiophenone, there is a video

And don't seem very complicated
 

Chemdog010297

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Can I do this synthesis at 140 Fahrenheit for 48 hours and get the same result ?
 
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