Vídeo de síntese do JWH-018

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Só há um problema: primeiro precisaremos produzir os seguintes produtos do zero!
Poderia me enviar o guia rápido para sintetizar o seguinte;
Indole 100 g;
1-Naphthoyl chloride 163 g;
TBAB (tetrabutylammonium bromide) 25 g;
1-Bromopentane 75 g;

Deveria ser fácil! 2/10 Difícil. Pffff


Este é mais fácil de fazer. 1/10 Dificuldade

5t0VyjwFHb
 

hydroman1212

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Olá, tenho uma pergunta
Há dois tipos diferentes de qualidade no precursor JWH-018 CHEAP e EXPENSIVE no mercado?
CAS 109555-87-5
3-(1-naftoil)indole
 

hydroman1212

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Se eu comprar 3-(1-naftoil)indole da China, ainda preciso purificá-lo (ETAPA 2) e depois passar para a ETAPA 3 (Síntese de JWH-018)?

 

G.Patton

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Sim, você está correto
 

rotovap5002

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"26. Um excesso de 1-bromopentano será evaporado em uma atmosfera (use ventilação adequada). O condensador de refluxo está instalado."

Por quanto tempo ele é deixado em refluxo depois que o condensador é instalado?
 

Chemlov007

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Por favor, ajudem! No estágio 1, meu produto se torna pegajoso e não cristaliza; depois de adicionar água destilada fria, ele fica assim. O que estou fazendo de errado?
SZTIplm02b
JtVxZh4Ww8

 
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G.Patton

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Olá, o JWH-018 pode ter a forma oleosa.
 

William Dampier

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Perhaps you used not enough solvent, if this is the first stage. Or you gave the mixture to warm up and the solvent evaporated.
 

Sintex

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Hello, can you tell me if it is possible to replace anhydrous aluminum chloride with anhydrous iron chloride at the first stage?
 

BalkanBoys

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Can you synthesise aluminum chloride by reacting amluminum foil with concentrated HCL ?
 

William Dampier

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If you take this topic, in the process of formation of the complex with AlCl3, HCl gas is released, you can saturate water or some other dry solvents.
 

Amynosha

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Hello, thank you for your videos. I wanted to ask how to make oily. I am asking because of the video of making hashish because you used jwh-018 oil in that clip. I would be very grateful if you could tell me.
Hello, thank you for your videos. I wanted to ask how to make oily. I am asking because of the video of making hashish because you used jwh-018 oil in that clip. I would be very grateful if you could tell me.
 

G.Patton

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This post about that. What exactly do u need?
 
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