Método de purificação de MDMA/ecstasy

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Olá amigos, obrigado pela contribuição, funciona muito bem, mas tenho uma dúvida, ao cristalizar (os cristais precipitam muito bem) não obtenho cristais como os típicos de mdma, é algo mais parecido com flocos de neve, com gelo congelado em um copo em um dia de neve, é vidro, mas muito frágil. Por que não consigo obter um vidro forte? Obrigado e saudações 😊
 

G.Patton

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Olá, de nada! Você usa uma geladeira para o procedimento de cristalização? Quanto mais rápido for o resfriamento, menores serão os cristais.
 
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Sim, é claro, primeiro eu deixo o produto de lado até que esteja em temperatura ambiente, então 15 ou 20% já estão cristalizados, depois coloco na geladeira por 2 horas e depois no freezer por 3 horas. Quase 100% do produto lavado cristaliza, mas os cristais são muito frágeis, quando manuseados para embalagem se transformam em areia
 

Mr Good Cat

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Fiz IPA algumas vezes e acho que esse estilo de cristal "areia" é uma propriedade natural da cristalização do IPA. Tente recristalizá-la em água para obter grandes cristais de rocha.
 
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Mr Good Cat

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O que notei é que o IPA é bom para remover o composto preto pegajoso, produto secundário da síntese.
 

William Dampier

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Large crystals are obtained with the inclusion of a water molecule. Therefore, sometimes it is better to use aq. HCl acid or add water additionally. You must begin crystallization at room temperature so that the process does not begin quickly. If you show a photo of your crystals, maybe I will tell you that you can change for this and get it in a larger size.
 

Keychainsaw

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I read heat makes it brown in here,
I had some issues with the hobby project. The sirup smelled like methylamine in the glass tray and im afraid there might be some methylamine hcl in the end product. Either way this looks fucked up and it looks like it doesnt want to dry any further. Acetone wash just usually turns it into a black tar. Have to say i forgot to dry it does the 4% aq make a bid difference?

This is what i managed to scrape together and kind of dry out. It tastes more salty than bitter. I dont know how methylamine hcl tastes but drying in the oven doesn't make it appear dryer. Its more tarlike than anything else. I'm ready to give up and just flush it. I did manage to get a whiter one with acetone wash but it has the same non bitter taste. Slightly salty. Could other salts have formed in the process? Maybe the aq layer was pipetted up aswell, in that case it might contain trace amounts of mercury?
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G.Patton

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Have you dried this in an oven? At what temp? I assume, there are not a lot of MDMA in this "product".
Looks looks dog shit.
 

Keychainsaw

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105 Celcius. I did manage to get a few gr of good stuff out it before with acetone washes it yielded only a few gr. Thanks for confirming to toss it than i stop wasting and experimenting on it. To be honest the taste test did not pass and it tasted salty and slightly metallic. It didnt want to dry or crash i will simply dump it. Thanks for the fast reply.
 
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