Síntese de metanfetamina a partir de efedrina usando I2 e H3PO2

hacke8

🥷 RESIDENT 🥷
New deal
Language
🇺🇸
Joined
Feb 26, 2024
Messages
133
Reaction score
42
Points
28
Senhores, fiz este experimento e o aqueci a 125 graus, porque o ácido fosfórico é aquecido a 130 graus, e haverá gás hidrogênio fosfato (tóxico). Há alguma maneira de evitar isso?
 
New deal
Language
🇺🇸
Joined
Jan 22, 2024
Messages
2
Reaction score
0
Points
1
isso funciona com pseudo?
 

Toti

🥷 RESIDENT 🥷
New deal
Language
🇺🇸
Joined
May 23, 2024
Messages
7
Reaction score
1
Points
3
Olá, há alguma diferença se eu usar sudoefedrina nessa receita?
Obrigado, senhor
 

amieri

🥷 RESIDENT 🥷
New deal
Language
🇺🇸
Joined
Jun 2, 2023
Messages
80
Reaction score
55
Points
18
You want a molar equivalent , these are hypothetical amounts, but say the the 6g of ephedrine is 20mmol of one mol of ephedrine then you'd want 20mmol equivalent of pseudo.im by no mean a pro and have never even looked up the molecular weight of either of them put that's the idea .
There's a post on here somewhere I believe from patten that is very detailed and informative about the subject definitely look it up because this is something that is very important in all reactions.
Sincerely B

!MAKE AMERICA COOK AGAIN!
 

kackbratze

Newbie
New deal
Language
🇩🇪
Joined
Jul 31, 2022
Messages
1
Reaction score
0
Points
1
Olá, tenho uma dúvida: em vez de iodo, poderia ser usado iodo potássico? Porque o iodo potássico é comprado com muito mais facilidade.
 

G.Patton

🐝SuperModerator
Expert
🥷 RESIDENT 🥷
New deal
Joined
Jul 5, 2021
Messages
3,334
Solutions
3
Reaction score
3,868
Points
113
Deals
Olá, não. Essas substâncias têm propriedades químicas diferentes.
 

CARLITOBRO

🥷 RESIDENT 🥷
New deal
Language
🇺🇸
Joined
Aug 24, 2024
Messages
47
Reaction score
33
Points
18
Posso usar ácido hidriódico 57% em vez de ácido hipofosforoso?
 

Bmth

🥷 RESIDENT 🥷
New deal
Language
🇺🇸
Joined
Aug 24, 2024
Messages
25
Reaction score
9
Points
3
Peça respostas a especialistas, pois não consegui e gastei muito dinheiro e materiais.
Bahasa Indonésia:Para esse estágio de destilação, o que é necessário para o próximo processo?
Bahasa Indonesia:Se o resultado do vapor da destilação ou o restante do material que é aquecidoSe o resultado do vapor da destilação ou o restante do material que é aquecido 🙏
 

Attachments

  • asn4K7uiJA.jpg
    asn4K7uiJA.jpg
    840.8 KB · Views: 151

Pinkbay

🥷 RESIDENT 🥷
New deal
Language
🇬🇧
Joined
Sep 20, 2024
Messages
23
Reaction score
7
Points
3
Professor, posso usar DCM sem destilação e ir diretamente para o cloreto de hidrogênio com excesso de peso?
 

William Dampier

🐝SuperModerator
Expert
🥷 RESIDENT 🥷
New deal
Joined
Jul 19, 2021
Messages
1,121
Reaction score
1,395
Points
113
You can do this, but it is better to extract into the water layer when acidification and evaporate part of the water. You can use aq. HCl
 
New deal
Language
🇺🇸
Joined
Sep 27, 2023
Messages
2
Reaction score
1
Points
1
Hello, please can you give the weights that can be followed with the steps to get one kilogram ?🙏
 

William Dampier

🐝SuperModerator
Expert
🥷 RESIDENT 🥷
New deal
Joined
Jul 19, 2021
Messages
1,121
Reaction score
1,395
Points
113
You must control the boiling to avoid problems with the volcano. Use boiling chips. Change the weight you need according to the specified proportions.
 

cicici

Newbie
New deal
Language
🇺🇸
Joined
Mar 21, 2025
Messages
2
Reaction score
0
Points
1
Hello, I have a question
I got a good result through this work
I have a few questions
1. It was heated to 100 degrees in hypophosphoric acid + ephedrine + iodine
There was a weight loss for the result. Would 110 degrees be okay?
2. Is it okay to calculate the capacity twice or three times for the mass production process and run the process? If so, how should we calculate the temperature and time of the reflux cooler?
3. I'm most curious about the process for number two. Simply put, if you start with six grams of ephedrine, if you put two or three times the dose in every process and manufacture it
I wonder what the temperature and time of the reflux cooler should be
4. The process of reflux cooler refers to the process in hypophosphoric acid + ephedrine + iodine
 

GhostChemist

🐝SuperModerator
Expert
🥷 RESIDENT 🥷
New deal
Joined
Nov 20, 2022
Messages
382
Reaction score
576
Points
93
The temperature can be 110 but longer in time
In this synthesis, phosphine is formed, therefore, an increase in the volume without ventilation hood is unsafe
 

cicici

Newbie
New deal
Language
🇺🇸
Joined
Mar 21, 2025
Messages
2
Reaction score
0
Points
1
Thank you for your answer
1. If you increase the volume, how much volume is appropriate?
2. If you increase the volume, how should you determine the time and temperature?
3. Why does it take longer than 100 degrees if you proceed to 110 degrees?
4.What is the appropriate temperature in your opinion?
 

kafka82

🥷 RESIDENT 🥷
New deal
Language
🇬🇧
Joined
Mar 23, 2025
Messages
29
Reaction score
2
Points
3
I am newbie - is there a video of this detailing the process? Also particualrly concerned about the best type equipment to procure fo rmagnetic heater and the reflux for example...
 

@speedboysss

Newbie
New deal
Language
🇺🇸
Joined
Apr 27, 2025
Messages
8
Reaction score
1
Points
1
Top