Alguns sais de anfetamina

[OneTensionSkyRed]

How is Amphetamine oxalate? Does anyone know about it's solubility? Some amine oxalates can be recrystallized from hot water so if Amph oxalate is similar in solubility this can be used to clean it easily.

Also which Amphetamine salts can be used for smoking without degrading when heated?

 

[GhostChemist]

Amphetamine oxalates maybe have low solubility, but this salt will be toxic for users

Some Amphetamine salts which are potentially can be used for smoking:

http://bbzzzsvqcrqtki6umym6itiixfhn...ads/amphetamine-salts-smoking-research.12460/

http://bbzzzsvqcrqtki6umym6itiixfhn...ia/amphetamine-salts-smoking-experiments.114/

 

[rampage]

i did a p2np al/hg amination to amphetamine, but when i finished i ended up with an oil, i did not gas it with hcl i just added hydrochloric acid with acetone and dripped it into rm until i reached a ph of 6, ive tried evaporating it and just end up with an oil, and i want to get amph hcl. any suggestions on what to do would be appreciated?

 

[GhostChemist]

Precipitation of an amphetamine with H2SO4 or H3PO4 give a powders.
But amphetamine with HCl solution with acidic pH (better 3-4) should be evaporated to precipitate and dried in desiccator contains NaOH

 

[rampage]

should i dissolve the oil in water and adjust ph or should i try and return it to amph freebase?

 

[GhostChemist]

You may carry out reaction in water with aqueous HCl

 

[GhostChemist]

Watch video and topic, I think this info will help with your question clearly
http://bbzzzsvqcrqtki6umym6itiixfhn...tion-to-amphetamine-using-i2-and-h3po2.12909/

http://bbzzzsvqcrqtki6umym6itiixfhn...tion-with-iodine-and-hypophosphoric-acid.117/

 

[rampage]

thanks mate

 

[rampage]

hey bro
i've added water to the oil and the oil dissolved straight away and alot of (what i'm assuming is amphetamine) fell out of solution, i checked the ph and it was 10.
should i get the ph down to 3-4 or 5-6, or will that affect the product that has just fallen out of solution?

 

[GhostChemist]

amphetamine FB has low solubility in water and can`t has high alkaline pH (in EtOH solution of AMP FB pH is ~8-8.5)
Use the Standard Amphetamine Test Strip for qualitative detect AMP
https://www.youtube.com/watch?v=_B8BmEsUAhw

 

[rampage]

thanks for your advice mate

 

[rampage]

this is the sulphate



and this is the hydrochloride

 

[William Dampier]

Amphetamine sulfate is the best choice, so it is used more. Even in pharmaceuticals. HCl salt is very hydroscopic.

 

[rampage]

yeah i found that out, dried it as much as i could then put it in the fridge.

 

[00mod00]

Very cool, I hope there are videos on the synthesis of xanthine derivatives.

 

[GhostChemist]

this topic dedicated Amphetamine Salts

 

[Robert Fico]

Tnx for such an interesting topic. do you have any idea about amphetamine sulphate solubility in ethyl alcohol?
I mean if instead of being dissolved in acetone base is dissolved in alcohol then h2so4 added?