Metóda purifikácie MDMA/ekstázy

[K53SK53S]

Dobrý deň, priatelia, ďakujem za príspevok, funguje to veľmi dobre, ale mám pochybnosť, pri kryštalizácii (kryštály sa veľmi dobre zrážajú) mi nevznikajú kryštáliky ako typické kryštáliky mdma, je to niečo podobné skôr snehovým vločkám, ľadovej námraze v pohári za zasneženého dňa, je to sklo, ale veľmi krehké. Prečo nemôžem získať silné sklo? Ďakujem a pozdravujem

 

[G.Patton]

Dobrý deň, nemáte za čo! Používate na postup kryštalizácie chladničku? Čím rýchlejšie chladenie, tým menšie kryštály.

 

[K53SK53S]

Áno, samozrejme, najprv ho nechám vonku, kým nemá izbovú teplotu, potom 15 alebo 20 % už vykryštalizovalo, potom ho dám na 2 hodiny do chladničky a potom na 3 hodiny do mrazničky. Takmer 100 % umytého výrobku vykryštalizuje, ale kryštáliky sú veľmi krehké, pri manipulácii s nimi sa zmenia na piesok.

 

[Mr Good Cat]

Niekoľkokrát som robil IPA a myslím, že tento "pieskový" štýl kryštálov je prirodzenou vlastnosťou kryštalizácie IPA. Skúste ju prekryštalizovať vo vode, aby ste získali veľké skalné kryštály.

 

[K53SK53S]

Vo vode? Ako to robíte takto, kamarát?

 

[Mr Good Cat]

http://bbzzzsvqcrqtki6umym6itiixfhni37ybtt7mkbjyxn2pgllzxf2qgyd.onion/threads/my-mdma-freebase-crystallization.5069/

 

[Mr Good Cat]

Čo som si všimol, IPA je dobrá na odstránenie lepkavej čiernej zlúčeniny, vedľajšieho produktu syntézy.

 

[William Dampier]

Large crystals are obtained with the inclusion of a water molecule. Therefore, sometimes it is better to use aq. HCl acid or add water additionally. You must begin crystallization at room temperature so that the process does not begin quickly. If you show a photo of your crystals, maybe I will tell you that you can change for this and get it in a larger size.

 

[Keychainsaw]

I read heat makes it brown in here,
I had some issues with the hobby project. The sirup smelled like methylamine in the glass tray and im afraid there might be some methylamine hcl in the end product. Either way this looks fucked up and it looks like it doesnt want to dry any further. Acetone wash just usually turns it into a black tar. Have to say i forgot to dry it does the 4% aq make a bid difference?

This is what i managed to scrape together and kind of dry out. It tastes more salty than bitter. I dont know how methylamine hcl tastes but drying in the oven doesn't make it appear dryer. Its more tarlike than anything else. I'm ready to give up and just flush it. I did manage to get a whiter one with acetone wash but it has the same non bitter taste. Slightly salty. Could other salts have formed in the process? Maybe the aq layer was pipetted up aswell, in that case it might contain trace amounts of mercury?

 

[G.Patton]

Have you dried this in an oven? At what temp? I assume, there are not a lot of MDMA in this "product".
Looks looks dog shit.

 

[Keychainsaw]

105 Celcius. I did manage to get a few gr of good stuff out it before with acetone washes it yielded only a few gr. Thanks for confirming to toss it than i stop wasting and experimenting on it. To be honest the taste test did not pass and it tasted salty and slightly metallic. It didnt want to dry or crash i will simply dump it. Thanks for the fast reply.