Metamfetamín z efedrínu pomocou jódu a červeného P

hacke8

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Ospravedlňujem sa, poslal som to opakovane.
 

TheNut22

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Môžem v tejto syntéze použiť len kryštály KI okrem tých jódových, neviete? Môžem z toho KI extrahovať jód, ale čo som sa dočítal ...
 

Anarchy Labz

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Prečo ste použili dcm, dá sa to urobiť aj bez dcm? Takisto nie je trochu veľa použiť 12 g I2 na 6 g efedrínu?
 

GhostChemist

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Môžete použiť petroléter, benzén alebo toluén
 

Bmth

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Ktorý je lepší zo všetkých námorníkov i Ktorý z týchto typov námorníkov je lepší v mojej krajine je ťažké nájsť
Indonézsky:
 

TheNut22

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Môžem namiesto DCM použiť xylén?
 

handle

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V akom štádiu by sa vytváral fosgén?
 

hacke8

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Nebude sa z neho vyrábať fosgén. Ak bude viac ako 130, vznikne plynný fosforovodík. Dávajte si na to pozor.
 
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TheNut22

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Áno! :). Keď robím túto syntézu, ak dám PVC hadicu z kondenzátora do plynového lapača plného uhličitanu sodného a aktívneho uhlia, čo môžem urobiť, aby som zabránil nasávaniu vodného roztoku z plynového lapača späť do reakčnej fľaše? Máte nejaké nápady, Handle?
 

rampage

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use a condom ontop of condenser
 

bigclit

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Môže mi niekto dať odkaz na metódu jedného hrnca, kde môžem získať všetky materiály osobne. Idc, ak skončím len s nejakým špinavým metamfetamínom, len hľadám projekt, kým je manželka na víkend mimo mesta.
 

Hypnou

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Duuuude prosím vás, nerobte to, naozaj existuje veľa lepších metód, čo sa môžete naučiť sami, len pre úctu k vareniu 🫠
 

iceberg

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Koľko ml má mať sklenený balónik a aký má byť spätný chladič? Môžete prosím odpovedať?
 

G.Patton

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O akom balóne hovoríte? Štandardný Allihnov spätný chladič, stredná veľkosť.
 

iceberg

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V zozname sa nachádza NH4Cl a H2SO4. Kde presne sa používajú pri syntéze? Ďakujem za odpoveď.
 

micked24

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Ammonium Chloride and Sulfuric Acid are combined to produce Hydrogen Chloride. Which is a gas that is used to turn the freebase into a hydrochloride salt. It is used towards the end of the video.
 

TheNut22

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Môžem namiesto DCM použiť xylén?
 

TheNut22

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No myslím si, že sa mi to podarí.
 

GhostChemist

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if o-xylene this is bad idea (B.P. 144C)
better petroleum ether, diethyl ether, benzene, toluene etc.
 

Pinkbay

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Ak pri výrobe voľnej zásady pridám vodu a hcl na okyslenie voľnej zásady, oddelím vrstvu vody a vodu úplne odparím, objaví sa na konci soľ? Teoreticky nie je potrebný chlorovodík?
 

GhostChemist

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When the free base extracted with DCM, you can use aqueous HCl for obtain salt after evaporation
 

rampage

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can phenylpropanolamine be used instead of ephedrine in this synth?
 

William D.

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Yes. If you have a supplier, send me a DM. The only problem is that the yield may be less than with the methylated version.
 

Chemtrail

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Seen that chemical on an Asian (India) chemical company for good price

Think that chemical is being used as an animal dog medicine
 

Chemtrail

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Swim had done this "red, white, blue" process with 6g E, 6g I, 3 g Rp and a couple of mls of D-H20 in a heat proof Corona beer glass bottle as a RXN vessel, a rubber stopper with airleak-proof connection with 5 foot tubing vertical and a punch balloon as a condenser, used a portable rice cooker & sand bath as heat source ~100-120C for 24 hours

Long Wet Reaction

Off heat to cool. Add 100 ml D-H20 . Filter Rp (**WASH OUT THE RP WITH HOT ACID, HOT ALCOHOL, HOT ACETONE, lukewarm water** good as new)
Add NaOH base solution till pH 12 A WHITE SLURRY WILL APPEAR
Extract with a NP fuel several times
Wash NP fuel/chilli with baking soda solution and then a D-H20 wash
Dry with drying agent for minutes and filter

Get a shot glass of D-H20 and drop 2-3 drops of HCl (or sulfuric acid) in it. Put this shot glass water with the NP/chilli and shake

Repeat several times

Extract water/chilli and evaporate on LOW heat

Speed a few hundred milligrams but good



* Swim got a VERY small percent yeild doing this method :(

Why did swim with 6 G of pseudoephedrine ended up with just a few hundred milligrams of speed ?! :(
 

Chemdog010297

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Can we get a synthesis of two for propiophenone ?
 

Chemtrail

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Think you can make synthetic Ephedrine from propiophenone, there is a video

And don't seem very complicated
 

Chemdog010297

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Can I do this synthesis at 140 Fahrenheit for 48 hours and get the same result ?
 
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