Syntéza oleja PMK z PMK (CAS 28578-16-7 vosková forma) vo veľkom meradle

[Curiousonion]

No táto metóda je určená pre pmk CAS 28578-16. Takže to môžete získať vo forme prášku, ktorý sa potom po ukončení reakcie zmení na olej.
Ale zdá sa to byť mimoriadne jednoduché, skúšal to niekto?

 

[C14]

It is bullshit from powder pmk dont work

 

[G.Patton]

This post is a good explanation, which was posted @btcboss2022 (thank you). I confirm, that it is a proven and working method.

 

[C14]

Hello the pmk powder gkyciate got one special smell?? Maybe i.got fake pmk

 

[ukises]

Hello Funciona.para el pmk ethyl powder???

 

[C14]

Your methode Dont work for pmk powder

 

[G.Patton]

Hello, the method in this topic work for PMK methyl glycidate as well

 

[C14]

Methyl , but really for pmk ethyl powder dont work,thanks

 

[Jordan Belfort]

You mean that dark pmk powder with only desolved with ethanol/alcohol @C14

 

[G.Patton]

Are you sure that you have PMK ethyl glycidate?

 

[C14]

Really now not sure, i am cheking my pmk powder dont have any smell , i mean odor, it is neutro

 

[G.Patton]

It's not a test, check its melting point and compare with a literature data.

 

[C14]

If is oil pmk, how i can know if is original or not?

 

[G.Patton]

I'm talking about its precursor PMK methyl glycidate. P2P can be checked by its boiling point, density.

 

[C14]

Hello meting point is 66 degrees c ?. Dificul find this information, thanks

 

[btcboss2022]

IF
Ak ste postupovali krok za krokom, mali by ste mať 2 vrstvy, vysvetlite mi bod po bode, čo presne robíte

 

[C14]

Hello i got pmk.glicidate i dont know exactly cas number, but is white not shinning , it is fatty , In water in ph 10, i cooked 2 times with naoh and hcl but after i use hcl start precipitatie white powder again, i think that is not.necesary use naoh becouse the ph is alcal ine, you got any idea?

 

[Win Win]

Dobrý deň, pane, môžem použiť túto metódu
1. K 100 g prášku PMK pridajte 100 ml etanolu a potom pridajte 100 ml destilovanej vody a potom uzavrite a miešajte pri izbovej teplote 90 minút, kým sa z neho nestane malý prášok.
2. Prefiltrujte kvapalinu (odvážte prášok) a pridajte kyselinu chlorovodíkovú v pomere 1:2.
3. Prášok nasypte do reakčnej nádoby, pridajte kyselinu chlorovodíkovú, začnite miešať, zvýšte teplotu na 75 stupňov a miešajte 3 hodiny. Uvidíte tmavú olejovitú látku.
4. Olej vyberte a použite ho v ďalšom kroku.

 

[C14]

Hello for 100 grms pmk, how many grams of hcl? Thanks

 

[C14]

Hello Hcl radio 1:2 you mean 100 gr pmk and 200 gram hcl?

 

[realboss]

. Add 3.25kg of HCL 37% in small portions, once all added keep the mixture at 80 °C reflux during 1 h stirring.
hcl 37% water solution ?

 

[C14]

Hello for what use.the s bicarbonate, for clean or.for change ph?

 

[Jordan Belfort]

Both, and probably some NaCl will be formed if aquous HCL has been used, resulting in general better kinetics (if minor trace stays in the oil).

 

[G.Patton]

It's need to carry out alkaline hydrolysis of ester.

 

[C14]

Hello , this one Add 3.25kg of HCL 37% pure. Not with something water? Thanks