Kristalizacija mefedrona (4MMC)

Khaafii

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Za najhitrejši način pridobivanja kristalov morate dati raztopino s 4MMC v zamrzovalnik, kar je najhitrejši način za pridobitev kristalov, vendar bodo ti majhni.
 

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Tehnika kristalizacije na rotacijskem uparjalniku (vedno nastane drobna frakcija).
 

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1 dam 1 ml vode za 1 g prahu skuham in pustim zaprto v hladilniku, ko odprem, se po 1 dnevu nič ne kristalizira.
To je treba odpreti ali zapreti in počakati, katera metoda je dobra
 

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Seveda se ne bo izkristaliziral. Vodo morate izhlapeti. Raztopino pustite pri sobni temperaturi in pustite, da voda izhlapi
 

subzero013

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Povejte mi o kristalizaciji v slanici, kako ločiti natrijev ali kalcijev klorid od mefedrona? V vašem glavnem prispevku o tem ni nobenih informacij.
 

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Zakaj morate uporabiti to nenavadno metodo? Videti je umazana in neučinkovita. Verjetno vam lahko pomagam z nasvetom? Kaj želite storiti?
 

whitelabel

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Any way to get brown or cream color "cakes" from 4mmc hcl not just crystals. Brown/cream color slabs or cakes about 2 to ,3 inches thick that have crystals in and around the pieces, these slabs hold their form once solidified and dried and do not crumble. I will be obliged for any knowledge regarding this 4mmc crystallization form and procedure if you have encountered such crystal slabs or cakes 🍰
 

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How it's possible? Apply more force to do it. To be honest, I don't clearly understand what is a problem.
 

Dr. MMX

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I believe that if powder required rinsing with acetone to get rid of unwanted, they could potentiall grow "harder" later on. I cant say its confirmed but its very wierd that exactly 3 cases were like that and otherwise its instantly crushing :)
 

subzero013

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Zanima me metoda kristalizacije pri negativnih temperaturah. Kristalizacija v vodi pri temperaturi minus 8 stopinj se mi je zdela zanimiva, le da zdaj nisem našel zamrzovalne komore, pri temperaturi minus 10 stopinj pa voda sama zamrzne. Tukaj je fotografija izdelka, pridobljenega s to metodo (po navedbah avtorja) - http://bbzazvqcrqtki6umyxfhni37ybttt7mkbjyxn2pgllzxf2qgyd.onion/atzccw56nma-jpeg.7537/ Ni mi pomembno, kakšne velikosti bodo kristali, glavno je, da proces poteka v hladilniku/zamrzovalniku ali v vakuumu. Ali lahko poveste kaj preverjenega in učinkovitega?
 

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Neveljavna povezava
Na voljo je več metod z jasno razlago. Ali potrebujete še kaj drugega?
 

subzero013

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tukaj je fotografija kristalov na tej povezavi.
 

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Which procedure make this bro.
 
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ChemDamn

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0Q8MifY2lF
 

ChemDamn

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tukaj je moj rezultat s to metodo. metoda je precej preprosta in hitra. vendar NaCl ali CaCl tu sploh nista potrebna. vse, kar potrebujete, sta voda in 4-mmc. vodo zavrite in v njej raztopite 4-mmc (1 g na 1 ml). nadaljujte z vrenjem, dokler površine raztopine ne prekrije film. nato raztopino prelijte v stekleno posodo s plastjo ~ 5 cm in jo pustite popolnoma pri miru 10 ur. To sem naredil pri sobni temperaturi + 8C. po 10 urah so kristali pripravljeni.
 

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in to je še ena metoda. raztopite 4-mmc v vodki 1 g na 2,5 ml. in pozabite na raztopino za 4-5 tednov pri sobni temperaturi. vodka izhlapi, kristali ostanejo v posodi
 

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minus temperatura ni pogoj. enako lahko storite pri temperaturi + 20C. vendar višja kot je temperatura v prostoru, več 4-mmc bo ostalo v matični raztopini. pri -8C bo skoraj ves 4-mmc izpadel iz raztopine. pri + 20C bo izpadlo približno 70 %, približno 30 % bo ostalo v vodi. kaj pa vam preprečuje, da bi vodo pregnali in dobili ostanke 4-mmc ter nato postopek kristalizacije ponovili znova?
 

subzero013

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Za 4-5 tednov je predolg, kristal je vsekakor odličen. Ste za kristalizacijo poskusili uporabiti sušilno peč/komoro? Lahko se izkaže, da boste z njo dosegli takšen rezultat, le da v krajšem času.
 

Didi

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izhlapevanje mora biti počasno, počasneje kot je, boljši in večji so kristali. ko uporabite sušilnik, potem boste dobili kristalni prah
 

Didi

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1 teden
 

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