2-iodo-1-p-tolyl-propan-1-one CAS:236117-38-7
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Mephedrone synthesis from 2-iodo-4'-methylpropiophenone (CAS 236117-38-7) with ethyl acetate
https://bbgate.com/threads/mephedrone-4-mmc-synthesis-from-haloketone-in-ethyl-acetate-1-10-kg-scale.39/
4'-methylpropiophenone iodination with iodine/cooper (II) oxide
https://bbgate.com/threads/iodination-of-4-methylpropiophenone-with-iodine-cooper-ii-oxide-large-scale.218/
Reaction scheme:
Reagents:
4'-Methylpropiophenone (cas 5337-93-9) 5 kg;
Сooper(II) oxide (CuO) 2.7 kg;
Isopropyl alcohol (IPA) 50 l;
Iodine 6.5 kg;
Equipment and glassware:
100 L Batch reactor, which is equipped with drip funnel, top stirrer, thermometer, temperature control system...