synthesis

  1. KokosDreams

    Question regarding amphetamine synthesis via P2NP + NabH4/CuCL2

    Hey folks, going through my notes (read below) I am wondering about three main questions right now: My questions now are: What PH do I need to bring the reaction to before adding DCM? Is it necessary to extract the aqueous phase with IPA or can I just extract with DCM and distill after...
  2. S

    EU SPEED PASTE ---> METH ?

    Question 
    is this the easiest way to make meth cheap (in EU) for personal quantities? is it possible to get D-METH or only racemic? will this synthesis http://bbzzzsvqcrqtki6umym6itiixfhn...hamphetamine-synthesis-from-amphetamine.1671/ work? i assume the speed paste would need to get washed, is it...
  3. KokosDreams

    Recrystalization of P2NP

    Question 
    Hey folks, as I am ordering my first P2NP soon I am looking for advice for the following subject: Recrystalization of P2NP I have read some things about this process in the forum and understood that it is recommended not only proof the quality of the P2NP but also to improve it's quality if...
  4. 2-Bromo-4'-methylpropiophenone synthesis from 4'-methylpropiophenone

    2-Bromo-4'-methylpropiophenone synthesis from 4'-methylpropiophenone

    2-Bromo-4'-methylpropiophenone synthesis (CAS 1451-82-7) from 4'-methylpropiophenone with HBr/H2O2 https://bbgate.com/threads/bromination-of-4-methylpropiophenone-with-hbr-h2o2-large-scale.215/
  5. Mephedrone synthesis

    Mephedrone synthesis

    Mephedrone synthesis from 2-iodo-4'-methylpropiophenone (CAS 236117-38-7) with ethyl acetate https://bbgate.com/threads/mephedrone-4-mmc-synthesis-from-haloketone-in-ethyl-acetate-1-10-kg-scale.39/
  6. Mescaline and TMA synthesis (and analogues). Video manual.

    Mescaline and TMA synthesis (and analogues). Video manual.

    This method is suitable for the syntheses of Mescaline and its analogues. https://bbgate.com/threads/video-synthesis-of-mescaline-and-analogues.3390/
  7. chemden

    Methods to synthesis Amphetamine

    I'm looking for a method to synthesize amphetamine in my laboratory. I have a chemistry degree, but almost no experience. This is why I don't know which synthesis method to choose. It would be helpful if some of you that have experience in this field could describe or refer to synthesis...
  8. 2-Bromovalerophenone synthesis from valerophenone

    2-Bromovalerophenone synthesis from valerophenone

    Valerophenone halogenation (CAS 1009-14-9) to 2-Bromovalerophenone (CAS 49851-31-2) https://bbgate.com/threads/synthesis-of-alpha-pvp-1-10kg-scale.12/
  9. α-PVP/MDPV synthesis from 2-Bromovalerophenone

    α-PVP/MDPV synthesis from 2-Bromovalerophenone

    α-PVP hydrochloride synthesis from 2-Bromovalerophenone (cas 49851-31-2) https://bbgate.com/threads/synthesis-of-alpha-pvp-1-10kg-scale.12/
  10. A

    MDMA synthesis validation & questions

    Hey everyone, I have some questions about this patchwork synthesis for moon rock that I would like some expert feedback and opinions, as well as answers to the following questions below: a) Is this procedure doable with the procedures and equipment mentioned below, and if so, what are some...
  11. M

    neutralization of amphetamine free base to amphetamine sulfate. questions and answers that may be bothering you.

    Hello everyone . the thread was created due to the fact that I have a few unanswered questions. questions : 1.should amphetamine free base (oil) be mixed with a solvent toluene / dcm etc before neutralization? if so, in what proportions? 20-30% of the oil volume will be OK? 2. in what ratio...
  12. 2-Iodo-4'-methylpropiophenone synthesis from 4'-methylpropiophenone

    2-Iodo-4'-methylpropiophenone synthesis from 4'-methylpropiophenone

    4'-methylpropiophenone iodination with iodine/cooper (II) oxide https://bbgate.com/threads/iodination-of-4-methylpropiophenone-with-iodine-cooper-ii-oxide-large-scale.218/
  13. DET synthesis (and analogues DMT, DiPT, MiPT) from indole via LiAH

    DET synthesis (and analogues DMT, DiPT, MiPT) from indole via LiAH

    https://bbgate.com/threads/video-synthesis-of-det-and-analogues-dmt-dipt-mipt-from-indole-via-liah.1400/
  14. D

    Problems with Labdas Heroin synthesis?

    Hello, I stumbled across this synthesis manual and I have a few questions to it. Though it is in german, maybe you can translate it... Synthese: In einem 10-ml-Zentrifugenglas werden 28,5 mg Morphin, 29,4 mg N,N-(Dimethylamino)-pyridin, 1 ml Dichlormethan (DCM) und 100 µ l Essigsäureanhydrid...
  15. G.Patton

    Syntheses of 2C-phenylethylamines

    Introduction 2C (2C-x) is a general name for the family of psychedelic phenethylamines containing methoxy groups on the 2 and 5 positions of a benzene ring. Most of these compounds also carry lipophilic substituents at the 4 positions, usually resulting in more potent and more metabolically...
  16. dark_side_of_chemistry

    calculation of proportions example of mephedrone synthesis

    Hello all . in this thread I would like to present the basics of calculating proportions on the example of mephedrone synthesis calculations. at the very beginning I will start with the fact that proportion counting is one of the main steps before starting work when carrying out any laboratory...
  17. Novator

    DET synthesis (and analogues DMT, DiPT, MiPT) from indole via LiAH. Video manual.

    ✅The technique is suitable for the synthesis of popular tryptamines from TIHKAL. For example, replacing diethylamine on dimethylamine (3:20), you will receive DMT. ⚠️The air temperature in the laboratory should not exceed 10°C. ☣️Exhaust ventilation, respiratory and eye protection.
  18. K

    4-AcO-DMT from Psylocibe Extraction?

    Is there a method for this synthesis? Thanks
  19. K

    2C-E Synthesis Method?

    Hi! Is there any improved 2c-e synthesis method to produce it on large scale? Is it possible to do it with regents that can be found on china suppliers? Thanks!
  20. I

    finding Equipment

    i plan to synthesis jwh 018 and im setting up new lab i need Equipments: Flask 1L-5L-10L Beakers 0,2-0,5-1L Silicone Baking Molds. Respirator mask Funnel for bulk materials
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