synthesis

  1. dark_side_of_chemistry

    calculation of proportions example of mephedrone synthesis

    Hello all . in this thread I would like to present the basics of calculating proportions on the example of mephedrone synthesis calculations. at the very beginning I will start with the fact that proportion counting is one of the main steps before starting work when carrying out any laboratory...
  2. Novator

    DET synthesis (and analogues DMT, DiPT, MiPT) from indole via LiAH. Video manual.

    ✅The technique is suitable for the synthesis of popular tryptamines from TIHKAL. For example, replacing diethylamine on dimethylamine (3:20), you will receive DMT. ⚠️The air temperature in the laboratory should not exceed 10°C. ☣️Exhaust ventilation, respiratory and eye protection.
  3. K

    4-AcO-DMT from Psylocibe Extraction?

    Is there a method for this synthesis? Thanks
  4. K

    2C-E Synthesis Method?

    Hi! Is there any improved 2c-e synthesis method to produce it on large scale? Is it possible to do it with regents that can be found on china suppliers? Thanks!
  5. I

    finding Equipment

    i plan to synthesis jwh 018 and im setting up new lab i need Equipments: Flask 1L-5L-10L Beakers 0,2-0,5-1L Silicone Baking Molds. Respirator mask Funnel for bulk materials
  6. dark_side_of_chemistry

    own idea for studios (lab specialization: mef production)

    Hello everyone, today I would like to share with you my idea for studios. I will try to gradually develop and add new ideas. Hope you also share your solutions and ideas. after all "two heads are more than one" 1. preliminary design of the laboratory. 2. Reaction vessel: 3...
  7. rickyrick

    5cl synthesis kits china

    Hi i heard that the chinese have been selling almost finished synthesis products of 5cl and other banned cannabinoids to circumvent the bans.So only finishing touches needed from end customer to make the chem.I cant find other info on this has anyone heard anyithing about it?I have asked my...
  8. dark_side_of_chemistry

    new idea for a mephedrone synthesis device from the recipe: Mephedrone synthesis in the NMP (large scale)

    Yo . I came up with another idea how to build a synthesis device ... (for mephedrone synthesis in nmp) thanks to the gravitational flow of the liquid we are able to divide the solution after the reaction (right after the methylamination is finished). Thanks to this, in tanks of this capacity...
  9. dark_side_of_chemistry

    construction of a fake mephedrone synthesis reactor. own idea

    Hello, I have an idea to build such a tank for mephedrone synthesis .. what do you think, can you advise something, what to change? hardware description: conical tank 115l. attach the stirrer to the top cover, make a hole for an additional substance inlet, install a reflux condenser and a...
  10. U

    easiest small scale cook set up at home

    Looking for a synthesis technique using most readily available products. Just enjoy playing in the kitchen and am looking to produce small amounts. I have successfully synthesized DMT and several THC concentrates, so I am not totally a beginner, but not far off either. Anyone able to point me...
  11. MethSpawner

    Recommend a method for first time METH synthesis,got all em reagents!

    Greetings fellow hiveminds! I will be starting my journey to meth cooking soon.I got access to most of the needed reagents like ephedrine,pseudo, red p,methylamine and p2p.Issue is I got little to no chemical knowledge and this will be my first synthesis.Do you guys think this is doable for...
  12. S

    Amphetamine Synthesis P2NP

    Hi, how much amphetamine I can synthesis from 1kg of P2NP?
  13. D

    Chloral Hydrate Synthesis

    Thought I share this Chloral Hydrate Synthesis route I found on the web once, which is a quite enjoyable, early sleeping aid. Needed: - anhydrous ethyl alcohol - concentrated hydrochloric acid (how concentrated?) - calcium hypochlorite Pour pure anhydrous ethyl alcohol into a large flask and...
  14. G.Patton

    Nitrazepam and 2-amino-5-nitrobenzophenone syntheses

    Introduction This method is presented the opportunity of Nitrazepam and 2-amino-5-nitrobenzophenone syntheses (also known as Mogadon; 7-nitro-5-phenyl-1,3-dihydro-1,4-benzodiazepin-2-one). There are two different ways of 2-amino-5-nitrobenzophenone, which have different precursors and levels of...
  15. R

    Procuring Coca Leaves

    Not looking for a link/source, unless thats allowed? (not sure what the rules are here on that) Is it feasible from within the US? I'm aware that the yield is something like 0.5% the mass of dried leaves, but I'm intrigued by the prospect of having such a pure product. Has anybody tried the...
  16. G.Patton

    Methoxetamine (MXE) synthesis

    Introduction Methoxetamine (also known as MXE, 3-MeO-2-Oxo-PCE, 2-(ethylamino)-2-(3-methoxyphenyl)cyclohexan-1-one) is an arylcyclohexylamine and a derivative of eticyclidine (PCE). It can also be thought of as the β-Keto-derivative of 3-methoxyeticyclidine (3-MeO-PCE), or the N-ethyl homologue...
  17. G.Patton

    Benzaldehyde synthesis from benzyl alcohol

    Introduction The procedure below describes the oxidation of benzyl alcohol to benzaldehyde in high yield using aqueous nitric acid as an oxidizer. Other methods of oxidizing benzyl alcohol to benzaldehyde are well-known, including those using chlorochromates, persulfate, or activated manganese...
  18. G.Patton

    Grignard Reagents

    Reactions with Grignard Reagents. A Grignard reagent has a formula RMgX where X is a halogen, and R is an alkyl or aryl (based on a benzene ring) group. For the purposes of this topic, we shall take R to be an alkyl group (e.g., BuMgBr). Grignard reagents are made by adding the halogenoalkane to...
  19. WillD

    Alpha-PVP synthesis (1-10kg scale). Complete video tutorial.

    Introduction This topic is represented alpha-PVP synthesis way in a medium scale 1-10 kg. There are elaborated video tutorials, which are allowed to produce this substance to anybody. Also, you can find here a list of necessary equipment and reagents. Equipment and glassware: Round bottom...
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