synthesis

  1. chemden

    Methods to synthesis Amphetamine

    I'm looking for a method to synthesize amphetamine in my laboratory. I have a chemistry degree, but almost no experience. This is why I don't know which synthesis method to choose. It would be helpful if some of you that have experience in this field could describe or refer to synthesis...
  2. 2-Bromovalerophenone synthesis from valerophenone

    2-Bromovalerophenone synthesis from valerophenone

    Valerophenone halogenation (CAS 1009-14-9) to 2-Bromovalerophenone (CAS 49851-31-2) https://bbgate.com/threads/synthesis-of-alpha-pvp-1-10kg-scale.12/
  3. α-PVP/MDPV synthesis from 2-Bromovalerophenone

    α-PVP/MDPV synthesis from 2-Bromovalerophenone

    α-PVP hydrochloride synthesis from 2-Bromovalerophenone (cas 49851-31-2) https://bbgate.com/threads/synthesis-of-alpha-pvp-1-10kg-scale.12/
  4. A

    MDMA synthesis validation & questions

    Hey everyone, I have some questions about this patchwork synthesis for moon rock that I would like some expert feedback and opinions, as well as answers to the following questions below: a) Is this procedure doable with the procedures and equipment mentioned below, and if so, what are some...
  5. M

    neutralization of amphetamine free base to amphetamine sulfate. questions and answers that may be bothering you.

    Hello everyone . the thread was created due to the fact that I have a few unanswered questions. questions : 1.should amphetamine free base (oil) be mixed with a solvent toluene / dcm etc before neutralization? if so, in what proportions? 20-30% of the oil volume will be OK? 2. in what ratio...
  6. 2-Iodo-4'-methylpropiophenone synthesis from 4'-methylpropiophenone

    2-Iodo-4'-methylpropiophenone synthesis from 4'-methylpropiophenone

    4'-methylpropiophenone iodination with iodine/cooper (II) oxide https://bbgate.com/threads/iodination-of-4-methylpropiophenone-with-iodine-cooper-ii-oxide-large-scale.218/
  7. DET synthesis (and analogues DMT, DiPT, MiPT) from indole via LiAH

    DET synthesis (and analogues DMT, DiPT, MiPT) from indole via LiAH

    https://bbgate.com/threads/video-synthesis-of-det-and-analogues-dmt-dipt-mipt-from-indole-via-liah.1400/
  8. D

    Problems with Labdas Heroin synthesis?

    Hello, I stumbled across this synthesis manual and I have a few questions to it. Though it is in german, maybe you can translate it... Synthese: In einem 10-ml-Zentrifugenglas werden 28,5 mg Morphin, 29,4 mg N,N-(Dimethylamino)-pyridin, 1 ml Dichlormethan (DCM) und 100 µ l Essigsäureanhydrid...
  9. G.Patton

    Syntheses of 2C-phenylethylamines

    Introduction 2C (2C-x) is a general name for the family of psychedelic phenethylamines containing methoxy groups on the 2 and 5 positions of a benzene ring. Most of these compounds also carry lipophilic substituents at the 4 positions, usually resulting in more potent and more metabolically...
  10. dark_side_of_chemistry

    calculation of proportions example of mephedrone synthesis

    Hello all . in this thread I would like to present the basics of calculating proportions on the example of mephedrone synthesis calculations. at the very beginning I will start with the fact that proportion counting is one of the main steps before starting work when carrying out any laboratory...
  11. Novator

    DET synthesis (and analogues DMT, DiPT, MiPT) from indole via LiAH. Video manual.

    ✅The technique is suitable for the synthesis of popular tryptamines from TIHKAL. For example, replacing diethylamine on dimethylamine (3:20), you will receive DMT. ⚠️The air temperature in the laboratory should not exceed 10°C. ☣️Exhaust ventilation, respiratory and eye protection.
  12. K

    4-AcO-DMT from Psylocibe Extraction?

    Is there a method for this synthesis? Thanks
  13. K

    2C-E Synthesis Method?

    Hi! Is there any improved 2c-e synthesis method to produce it on large scale? Is it possible to do it with regents that can be found on china suppliers? Thanks!
  14. I

    finding Equipment

    i plan to synthesis jwh 018 and im setting up new lab i need Equipments: Flask 1L-5L-10L Beakers 0,2-0,5-1L Silicone Baking Molds. Respirator mask Funnel for bulk materials
  15. dark_side_of_chemistry

    own idea for studios (lab specialization: mef production)

    Hello everyone, today I would like to share with you my idea for studios. I will try to gradually develop and add new ideas. Hope you also share your solutions and ideas. after all "two heads are more than one" 1. preliminary design of the laboratory. 2. Reaction vessel: 3...
  16. rickyrick

    5cl synthesis kits china

    Hi i heard that the chinese have been selling almost finished synthesis products of 5cl and other banned cannabinoids to circumvent the bans.So only finishing touches needed from end customer to make the chem.I cant find other info on this has anyone heard anyithing about it?I have asked my...
  17. dark_side_of_chemistry

    new idea for a mephedrone synthesis device from the recipe: Mephedrone synthesis in the NMP (large scale)

    Yo . I came up with another idea how to build a synthesis device ... (for mephedrone synthesis in nmp) thanks to the gravitational flow of the liquid we are able to divide the solution after the reaction (right after the methylamination is finished). Thanks to this, in tanks of this capacity...
  18. dark_side_of_chemistry

    construction of a fake mephedrone synthesis reactor. own idea

    Hello, I have an idea to build such a tank for mephedrone synthesis .. what do you think, can you advise something, what to change? hardware description: conical tank 115l. attach the stirrer to the top cover, make a hole for an additional substance inlet, install a reflux condenser and a...
  19. U

    easiest small scale cook set up at home

    Looking for a synthesis technique using most readily available products. Just enjoy playing in the kitchen and am looking to produce small amounts. I have successfully synthesized DMT and several THC concentrates, so I am not totally a beginner, but not far off either. Anyone able to point me...
  20. MethSpawner

    Recommend a method for first time METH synthesis,got all em reagents!

    Greetings fellow hiveminds! I will be starting my journey to meth cooking soon.I got access to most of the needed reagents like ephedrine,pseudo, red p,methylamine and p2p.Issue is I got little to no chemical knowledge and this will be my first synthesis.Do you guys think this is doable for...
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