Thought I share this Chloral Hydrate Synthesis route I found on the web once, which is a quite enjoyable, early sleeping aid.
Needed:
- anhydrous ethyl alcohol
- concentrated hydrochloric acid (how concentrated?)
- calcium hypochlorite
Pour pure anhydrous ethyl alcohol into a large flask and...
Introduction
This method is presented the opportunity of Nitrazepam and 2-amino-5-nitrobenzophenone syntheses (also known as Mogadon; 7-nitro-5-phenyl-1,3-dihydro-1,4-benzodiazepin-2-one). There are two different ways of 2-amino-5-nitrobenzophenone, which have different precursors and levels of...
Not looking for a link/source, unless thats allowed? (not sure what the rules are here on that)
Is it feasible from within the US? I'm aware that the yield is something like 0.5% the mass of dried leaves, but I'm intrigued by the prospect of having such a pure product. Has anybody tried the...
Introduction
Methoxetamine (also known as MXE, 3-MeO-2-Oxo-PCE, 2-(ethylamino)-2-(3-methoxyphenyl)cyclohexan-1-one) is an arylcyclohexylamine and a derivative of eticyclidine (PCE). It can also be thought of as the β-Keto-derivative of 3-methoxyeticyclidine (3-MeO-PCE), or the N-ethyl homologue...
Introduction
The procedure below describes the oxidation of benzyl alcohol to benzaldehyde in high yield using aqueous nitric acid as an oxidizer. Other methods of oxidizing benzyl alcohol to benzaldehyde are well-known, including those using chlorochromates, persulfate, or activated manganese...
Reactions with Grignard Reagents.
A Grignard reagent has a formula RMgX where X is a halogen, and R is an alkyl or aryl (based on a benzene ring) group. For the purposes of this topic, we shall take R to be an alkyl group (e.g., BuMgBr). Grignard reagents are made by adding the halogenoalkane to...
Introduction
This topic is represented alpha-PVP synthesis way in a medium scale 1-10 kg. There are elaborated video tutorials, which are allowed to produce this substance to anybody. Also, you can find here a list of necessary equipment and reagents.
Equipment and glassware:
Round bottom...