3 cmc how to get this product

antrax

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How do I get simillar product to this ,there is a lot of it in Romania ,I haven't seen 3 cmc from forum to look like this
lexiihow much they sell for in romania street price per gram?
 

lexii

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breathing.fire

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What You mean how to buy or how to make structures like this
 

Bazooka90

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Spirou

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They throw to freebase acid HCl acetone and water and wait 2 weeks this all
eddycordonHi. How many water need around? And just put the freebase + aceton acid wich is ph5. After this just throw water?? And then need to wait to evaporate right? Pls help me how much water have to throw example if i use 1 kg 2br3ch.... Thanks for the answer
 

Jesse_Pinkman_

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so, my experience is,
100g 2b3c
300dcm
200methylamin40% aqua
3 hours stirring
I use a sealed glas 1,8l, put foil between lid and glass so that nothing smells or gas escapes.
After reaction took place
2 times washing with dest.water
1 time extract water phase with dcm
put into rm,
add same amount fresh water into rm
put on magnetic stirrer
acidificaction drop by drop till ph6, about 50-55ml HCI,
after that take the water layer,evaporate the, let it crystallize, takes some time
opt. rotovap till 50% of the water is gone, then air drop


ethylacetat is possible, takes only 20 min, no heating necessary, rest same prosedure like with dcm

I waited min 2 days untill crystals began to form, these on the picture have not been washed with acetone but after that they are like glass. Very nice
 

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PolandoEmingarnte

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so, my experience is,
100g 2b3c
300dcm
200methylamin40% aqua
3 hours stirring
I use a sealed glas 1,8l, put foil between lid and glass so that nothing smells or gas escapes.
After reaction took place
2 times washing with dest.water
1 time extract water phase with dcm
put into rm,
add same amount fresh water into rm
put on magnetic stirrer
acidificaction drop by drop till ph6, about 50-55ml HCI,
after that take the water layer,evaporate the, let it crystallize, takes some time
opt. rotovap till 50% of the water is gone, then air drop


ethylacetat is possible, takes only 20 min, no heating necessary, rest same prosedure like with dcm

I waited min 2 days untill crystals began to form, these on the picture have not been washed with acetone but after that they are like glass. Very nice
Jesse_Pinkman_how much u get form 100ml 2b3ch crystal 3cmc?? why is yellow ?
 
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Jesse_Pinkman_

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how much u get form 100ml 2b3ch crystal 3cmc?? why is yellow ?
PolandoEmingarnte2b3c is a yellow oil, some people sah they get a black oil but that makes no sense. Yeald is not good, about 20%
Maybe there are better ways to do this but i tried very different kind of synthesis and only this way gives me crystals like that. While acidificaction the RM becomes yellow and when it nears ph 6 its more orange but you only take the water layer, i tried to get someting from organic layer but nothing happened. Its rubbish
 

Jesse_Pinkman_

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This is how it should look like
 

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PolandoEmingarnte

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PolandoEmingarnte

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I can not say in public, if you need some i can order it for you, but will cost a little bit more, that price is just for me, you know. He will not give it to other people for this price
Jesse_Pinkman_ok understund
i get form poland for 150€ 1l 100km from my house in wroclaw in lab 2b3ch 2b4m 2b3m 2b4chl and 2bV.
But good to know u pay much more because u pay low price
 

Spirou

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Hi. How many water need around? And just put the freebase + aceton acid wich is ph5. After this just throw water?? And then need to wait to evaporate right? Pls help me how much water have to throw example if i use 1 kg 2br3ch.... Thanks for the answer
 

Jesse_Pinkman_

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Hi. How many water need around? And just put the freebase + aceton acid wich is ph5. After this just throw water?? And then need to wait to evaporate right? Pls help me how much water have to throw example if i use 1 kg 2br3ch.... Thanks for the answer
horv.helgaSame amount of water as rm.
I would do small steps, like 200g at one time ,not 1kg. If something goes wrong, you have a problem.
 
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