6CL-ADB-A (MDMB-5en-HENACA) solid product synthesis

[lutte123]

Anybody can help and share recipe how to prepare this noid?
I tried to follow 5CL recipe both methods - ice water quench or DCM extraction + EtOH crystalisation too but not able to get solid (crystals) product.
Precursor works very good with bromopentene, but with bromohexene always got just oil/sticky paste product.

 

[lutte123]

Brother what are you talking about? Your reply makes no sense for me