Amphetamine from P2P (phenyl-2-propanone)

[jokerr]

don't use toluene, it is not working at all .
I think steam destination is the best.
my black liquid transfer to a light yellow liquid.
but it takes a long time, and my first try was not so good.
I had only a little from 100ml black liquid.

my next try I use a 3 neck flask, I connect my pear shape separator funnel to it and fill with water.
slowly, dropwise, add the water to the flask where my black liquid is located.
every time the water connect with the black liquid, you get steam .
this steam reflux and collect it in a cylinder

SaulWhat is the result if I use petroleum ether?
Normal ether controlled liquid is not allowed to be sold in my country.

 

[Bartholomeus]

don't use toluene, it is not working at all .
I think steam destination is the best.
my black liquid transfer to a light yellow liquid.
but it takes a long time, and my first try was not so good.
I had only a little from 100ml black liquid.

my next try I use a 3 neck flask, I connect my pear shape separator funnel to it and fill with water.
slowly, dropwise, add the water to the flask where my black liquid is located.
every time the water connect with the black liquid, you get steam .
this steam reflux and collect it in a cylinder

Saul
After HCL hydrolisis, NaOH solution is added to it and steam distillation is made
Did you add NaOH after hydrolisis?
Can you show picture how does your yellow liquid look like?

 

[Saul]

Did you add NaOH after hydrolisis?

ChingShih yes I did and I also add methanol but this is not needed

 

[Saul]

http://bbzzzsvqcrqtki6umym6itiixfhni37ybtt7mkbjyxn2pgllzxf2qgyd.onion/attachments/lbcfyxhuxr-jpg.8207/?hash=e7ffa8dfeda7c69c4449d436ad1b8f63

 

[Saul]

What is the result if I use petroleum ether?
Normal ether controlled liquid is not allowed to be sold in my country.

jokerr
dont know my friend but different sources say DCM is the best

 

[Bartholomeus]

http://bbzzzsvqcrqtki6umym6itiixfhni37ybtt7mkbjyxn2pgllzxf2qgyd.onion/attachments/lbcfyxhuxr-jpg.8207/?hash=e7ffa8dfeda7c69c4449d436ad1b8f63

Saul
Looks like amphetamine freebase, does it smell nice?
Did you try to add sulfuric acid to this yellow looking oil?
I smell success

 

[Saul]

Looks like amphetamine freebase, does it smell nice?
Did you try to add sulfuric acid to this yellow looking oil?
I smell success

ChingShih
not yet soon I try

 

[Saul]

Looks like amphetamine freebase, does it smell nice?
Did you try to add sulfuric acid to this yellow looking oil?
I smell success

ChingShih
Bad news no reaction at all like my previous 4 fails

when all the water is removed from my light yellow substance, the pH is back 7
I try to wash with NaOH so pH is back 14 but when separated again pH is back 7
after add methanol1/1 and dropwise sulphuric acid zero reaction nothing
this is now the 5th time the last step fail

PS: my light yellow substance smelt very good

 

[Saul]

I still do not believe that someone succeeded in this syntheses.
no proofs posted from nobody

 

[UWe9o12jkied91d]

Saul my man, no offense but if you can't perform your steam distillation it's not the syntheses fault or people are not lying to you. According to your description you destroyed the freebase by heating it so much that water instantly evaporated, it is plain wrong what you did.If you care to stop improvising tried and tested techniques like steam distillation maybe you would get more results. Either add some clean water to the extracted portions in 1 vessel, or with 2 separate vessels, 1 for steam connected to the other one.

 

[flask]

Saul my man, no offense but if you can't perform your steam distillation it's not the syntheses fault or people are not lying to you. According to your description you destroyed the freebase by heating it so much that water instantly evaporated, it is plain wrong what you did.If you care to stop improvising tried and tested techniques like steam distillation maybe you would get more results. Either add some clean water to the extracted portions in 1 vessel, or with 2 separate vessels, 1 for steam connected to the other one.

UWe9o12jkied91dI also want to know how the steam destination work best and what to use for it

 

[UWe9o12jkied91d]

I also want to know how the steam destination work best and what to use for it

flask

Solvents recovery

Introduction In the synthesis of mephedrone (4-MMC) and other psychoactive substances at different stages (synthesis and purification) use different solvents, which are not entered into a chemical reaction. They remain in the same form as before syntheses. However, they are mixed with dirt, and...

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Steam Distillation

Introduction. Steam distillation is analogous to simple distillation, the main difference being that steam (or water) is used in the distilling flask along with the material to be distilled. Experimentally the setups are arranged more or less the same (Fig.1), with small differences being how...

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Decantation, gravity filtration and liquid transferring

Introduction. In this topic, I'll overview some important laboratory techniques. Hard to overestimate the useful and helpful importance of these operations. Decanting, gravity filtration and liquid transferring are simple but take some attention and a little laboratory skill. Practicing them is...

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[Camilo]

Will this work if I want to get MDA from M.D-phenylacetone? How does the proccess change? What can I do If I can afford the rotovap? Is there a video explaining the proccess? Sorry for all this questions, I am an undergraduate chemist that wants to start cooking

 

[G.Patton]

Will this work if I want to get MDA from M.D-phenylacetone? How does the proccess change? What can I do If I can afford the rotovap? Is there a video explaining the proccess? Sorry for all this questions, I am an undergraduate chemist that wants to start cooking

CamiloI recommend you to start from syntheses with video tutorials. You will stuck with numerous questions without any experience.

 

[Hank Schrader]

This is MDA obtained by the leucart reaction.
Good product with a pleasant aroma.
The most interesting thing is that the smell remains even after distillation and washing with acetone
This means that less than 1% of aromatic impurities give an intense smell to the product.

 

[Bartholomeus]

This is MDA obtained by the leucart reaction.
Good product with a pleasant aroma.
The most interesting thing is that the smell remains even after distillation and washing with acetone
This means that less than 1% of aromatic impurities give an intense smell to the product.

Hank SchraderNice rocks you obtained
You used mdp2p via formamide+formic acid to get mda? standard leuckart reaction?
Does ratios for leuckart amphetamine also work for leuckart mdma-mda reaction?

 

[Hank Schrader]

Nice rocks you obtained
You used mdp2p via formamide+formic acid to get mda? standard leuckart reaction?
Does ratios for leuckart amphetamine also work for leuckart mdma-mda reaction?

ChingShihConditions are different.
various hydrolysis.
MDMA and methamphetamine can be produced by the leucart reaction.
You need n-methylformamide.
To get huge yields - you must learn to understand the essence of the process and feel the reaction.

 

[Bartholomeus]

Conditions are different.
various hydrolysis.
MDMA and methamphetamine can be produced by the leucart reaction.
You need n-methylformamide.
To get huge yields - you must learn to understand the essence of the process and feel the reaction.

Hank SchraderWhat are the yield from MDMA and meth produced by leuckart? 800-900ml from 1L ketone?
What do you mean with various hydrolysis?
And what do you mean with the essence of the process?

 

[Hank Schrader]

What are the yield from MDMA and meth produced by leuckart? 800-900ml from 1L ketone?
What do you mean with various hydrolysis?
And what do you mean with the essence of the process?

ChingShih1180-1230g MDMA you can get from 1000mls MDP2P.

 

[Xiao hua]

What is aluminum grit. can share me whit aluminum grit formula.

 

[UWe9o12jkied91d]

What is aluminum grit. can share me whit aluminum grit formula.

Xiao huaAlumina used in dentistry is sufficient or foil

 

[UWe9o12jkied91d]

What chemical can instead

Xiao huaU dont have aluminium foil in china?

 

[Xiao hua]

U dont have aluminium foil in china?

UWe9o12jkied91dBut mercury chloride not available