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any 3CMC synthesis method?

Bazooka90

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I would like to know also about that
 

Selassi

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Yes im very curious too... Help would be greatly appreciated ofcourse
 

WillD

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What are your starting reagents?
 

Selassi

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Chloropropiophenone, but its the same route as with methylpropiophenone right?
 

Selassi

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2-bromo, 3-chloropropiophenone to be exact
 

Bazooka90

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If i am right, we can use the same method like for 4mmc synthesis, replacing 2-Bromo-4-Methylpropiophenone with 2-bromo, 3-chloropropiophenone?
 

dark_side_of_chemistry

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Exactly all bromoketones we do the same ... if we bromine a compound, then we carry out amincaje some amine. mostly using SN2 for this.
 

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If i am right, we can use the same method like for 4mmc synthesis, replacing 2-Bromo-4-Methylpropiophenone with 2-bromo, 3-chloropropiophenone?
Bazooka90You just need to recalculate the proportions a little, and some features of crystallization
 

Selassi

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You just need to recalculate the proportions a little, and some features of crystallization
William DampierOk ok... So cryssing is different, it will not fall out with HCl and tempreduction or how?

Couldnt find this post from SynthMaster which is quoted above
 

WillD

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In general, the process is almost the same for all replaced compounds, do not worry about it. If you have reagents, write in private messages, I will help with synthesis in detail.
 

Selassi

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You just need to recalculate the proportions a little, and some features of crystallization
William Dampier Which features do we need to change for crysallization? Does cmc crystallize with the freezermethod used in mmc-variants?
 

rafael1985

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Somebody can help with 3 cmc synthesis after acidification is still oil
 
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