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How did you do this? Can you describe your procedure?
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How did you do this? Can you describe your procedure?
pH is 2 really acid
5-5.5 is optimal pH but there is a lot of watery HCl acid and 3MMC salt precipitation would dissolve in water
What I must do try evaporate this water when I put to freezer nothing come.Or maybe put acetone and use freezer.Or maybe try put sodium carbonate make pH higher will be work?
You have to alkalize your solution to pH 12-13, extract 3MMC free base by ether or petroleum ether and than add HCl gas to acidify solution. You'll get 3MMC salt precipitate.
I make every steps like bromination 4 MMC on dichlorometane but I start from oil and after acidification i let in room temp and nothing come only water again somebody know how to make crystalization process?Is different like with 4 MMC
You have to alkalize your solution to pH 12-13, extract 3MMC free base by ether or petroleum ether and then add HCl gas to acidify solution. You'll get 3MMC salt precipitate.
my 3cmc yield is very brownish,does anybody know how to make it more white?can i use some bleach?
my 3cmc yield is very brownish,does anybody know how to make it more white?can i use some bleach?
I have problem to make powderAfter acidificarion is nothing come.I put to frezer with acetone nothing come after evaporate is Black gum.PH is good.With 4 MMC and 4 CMC was not problem.Can You help somehow?
my 3cmc yield is very brownish,does anybody know how to make it more white?can i use some bleach?
There is too much water, I think. You have to get rid of water. I told you how to deal with it.I have problem to make powderAfter acidificarion is nothing come.I put to frezer with acetone nothing come after evaporate is Black gum.PH is good.With 4 MMC and 4 CMC was not problem.Can You help somehow?
@Berlin777 check this out
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