Need help with Pmk ethyl glycidate to MDMA synthesis

[William D.]

What is this kind? There is a chance that you need to react with alkali before making rearrangement with acid

 

[C14]

Hello william which.pmk.glycidate.need one step only with hcl to.mdp2p??? Thanks

 

[strangerdanger]

Damn 90% yield is solid. I yielded 62% using 1:1 dh2o, add 10% naoh until ph 8, after 1 hour add conc hcl until co2 evoluton ceases then held at 75c for 3 hours.

What were the ratios of h2o and hcl did you use? Im wondering if my supplier sucks or my recipe is bad. I was able to get 75% using the old pmk glyc using the above recipe

 

[C14]

Dices que echastes naoh hasta ph 8 mI pmk powder tiene ph 10 sin echarle naoh, tienes alguna idea?

 

[strangerdanger]

the recipe you mentioned sounds very similar to this one....

glyc : dh2o : etoh at 1:1:1 ratios mixed for 1 hour, then hcl and reflux for 3 hours. Ive never tried that recipe myself so i dont know the yields

 

[chinacat]

Same synth. Skip a few steps.

 

[robinhood]

Are you sure of ratios?

This definitely was the recipe we followed - i appreciate your response.

 

[strangerdanger]

ive never tried it myself. im simply sharing a recipe that i think is similar to what youre asking for. Im sure there are other recipes using different ratios which is something youll have to figure out and see which one works best for you. I also shared my recipe that yielded 62% from the waxy solid which i think is simpler than the one using etoh. to each their own.

can you describe ur pmk? is it solid at room temp? color? dark brown light brown? i

 

[robinhood]

Thanks for sharing.

Yes its wax at room temp, i believe the color would be more on the lighter end of the color brown. It sort of looks like solidified honey.

 

[btcboss2022]

Hello,

I will receive a sample of CAS 285-16-7 and it's a yellowish liquid not wax:
View attachment 4026

So you test that ratios and it's worked?
glyc : dh2o : etoh at 1:1:1 ratios mixed for 1 hour, then hcl and reflux for 3 hours
What ratio of HCL?
Thanks

 

[robinhood]

This is the PMK wax i used. Im not sure if i succeeded on attaching a photo of the PMK wax i have. Its definitely light brown - golden color and is very much similiar to how solid, dry honey looks in a jar. The oil i yielded from the wax was a dark brown liquid. My yield 60%

 

[Gale]

is it ethanol used in the conversion or ethyl acetate?

 

[Unreacted Freebase]

ethanol

 

[Followme38]

Does anyone have luck with making good oil from this new pmk from china? Everybody is calling it a glycidate but its not anymore since china banned the ethyl glycidate last year, now they are selling a product what looks like a honey like substance when heated at 30 degrees celsius, and a cream white powder, the ethanol formula gives a dark honey like oil, it gets hard after it cools down. See video...hope anyone can shed on it and more info

 

[derick12sabreh]

Hello, i'm also new in this field. Can someone tell me the best way to get PMK poweder to Europe, and also production cost of MDMA? Thank you

 

[Followme38]

Powder or oil getting it is simple now cause the new pmk is not on any list so china sends it with ups at the moment, but its completly useless china does not share formula also, so conversion correctly first is key.

 

[derick12sabreh]

And what is good price for that? If someone will has also good tips about MDMA, here or PM, i will be grateful

 

[Followme38]

Price in china is now 160 usd bulk 150 usd delivered, but there is no use for buying yet cause extraction formula not available, myself including trying to figure out now for a month or so.