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LearnByPain666

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Hey i am new here ✌️
i have some Basic questions and will be glad to find some answers.

1.If i have theoretical 1L benzaldehyde, how much nitroethan and N-butulamine i need for this 1L? And is there a stronger Version of N-butulamine for better Reaktion?

2.its better to let it reakt alone without extra heat over a long time?

thank you for all Informations and tipps 🙏🏻
 

Osmosis Vanderwaal

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Based only on your description, this recipe makes nothing useful as far as I can tell Is it supposed to be valerophenone?
 

LearnByPain666

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Hey thanks for answer🙏🏻 wanna theoretikal do phenylnitropropene.
allready find this recipe here:

question is did i Need This 50ml GAA? And can i change isopropyl against methanol?

is there a stronger/more reaktive Version of n-butulamine?
  • Benzaldehyde - 200ml.
  • Nitroethane - 200ml
  • n-Butylamine - 20 ml
  • Glacial acetic acid (GAA) - 50 ml
  • Isopropyl alcohol (IPA)
 

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The ratio of benzaldehyde to mitroethane is off. The N-butylamine is being used as the base and you obably shouldn't try to change it. You don't have methanol in your ingredients, so it looks like you already swaapped it for iso, which is fne. You do need GAA, but you can't say how much until you determine how much nitro-alcohol you got from the Henry reaction you did first. you need ethyl acetate, or some other polar solvent extractant
 

SoldadoDeDrogas

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No, he wants to make p2np. I've been day dreaming about Henry for about a year now.
Just use the portions from the recipes where you got it from. I believe one of the experts posted a p2np via Henry condensation.. Just adjust it for proper ratio. Make sure you have molar equivalents if you are not dealing with %100 pure or substitute compounds.

The GAA is to keep byproducts from being formed or something. minimizes toxicity if I recall. I don't believe IPA is necessary for this, or any alcohol. For Henry you will need Benzaldehyde, NitroEthane and the amine. n-Butylamine or cyclohexlamine are the proposed amines for the recipe. They are hard to come by for some, but they give the best product/yield for what they're worth. It is rumored that other amines may work, methylamine, ethylamine. Allegedly ammonium acetate will work but I have not heard or know any other details.

If I were you I would not wait for answers here, rather I would take some initiative and look up everything you can about: Henry reaction/condensation for P2NP. Making Amphetamine via P2NP with mercury aluminum amalgam. (AlHg). You can always try to ask the Experts, that is what they are here for. Definitely check the forum threads and video section. There is definitely a video or two about this.

This isn't something you want to use extra heat or time. Do it exactly like it is instructed. You can even do it in small and quick batches with your microwave.
 

LearnByPain666

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🙏🏻 thank you for this honest answer 😎 yes you are right. Wanna do p2np. And as i remember from old times there was no gaa inside. But i am not a chemic or pro. So is 50/50 benzalyhyde —niroethan correckt? Or its Like 70/30? The iso is for Washing later with vacum Pump and Filter. I can get all of this things in pure Labor quallity. So of you have a tip for best results please let me know.
 

SoldadoDeDrogas

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Yes. I believe equal parts benzaldehyde/NitroE 1 to 1. n-butylamine or cyclohexylamine is about 1/5 of that portion I think? 100ml benz 100ml nitro and 20ml amine. Don't assume I am correct. I haven't done this. Go look it up from several sources. OK, so the IPA is for washing the P2NP. In that case you will want to make sure it is cold and anhydrous and pure as possible. You can use %99 IPA and add table salt to soak up any moisture and filter it out - epsom salt will dissolve in the IPA. And yeah, the GAA isn't 'NECESSARY' for the synthesis. Neither is cleaning the excess iodine in a red P cook, but you see the difference in meth made with this process versus krokodil made carelessly. You don't want your speed to start eating holes in peoples flesh and what not, I hope... If you wanna be a cook. Do everything as best to your ability, don't skip a step to wash or purify. Make yourself stand out by providing the BEST possible quality you can.
 

LearnByPain666

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🙏🏻thanks for this fast Info. Ofc only clean and pure Produkts. Quallty is always the winner on market. Today Theo Sell mostly coffein with metha and Minimum Amphetamin. This Business change into a reall crap Business.
 
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