Simple One-Pot Synthesis of NEP (N-Ethylpentedrone)

gomez420

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1. Will 30% Hydrogen Peroxide work (for step 4) instead of 35%?

2. How much RPM must be used for stirring to get optimal results?
 

A5kL3Pi0s

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+/-400-450, but depends on the stage of synthesis

if you dont have an addition funnel for example, it might be smarter to turn the sitrring down a bit while adding chemicals in to avoid splasshing, but I guess thats common sense anyway 🤷‍♂️
 

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also you can go higher aswell, shouldnt hurt the reaction
if u stir too slowly maybe upper part in the beaker wont get mixed enough/at all, so keep that in mind....
ooor use a reactor with overhead stirrer haha
 

Dexterror

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Does someone do it without heating ? how long it take ?
 
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