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[TUTORIAL] How to make LSD #2

Gusfring666

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Extraction of Amides from Lysergic Acid: Start with Morning Glory national seeds, the young seeds of the Hawaiian wooden baby Rose, ergot cultured or naturally ergot compounds occurring.

NOTE: Morning glory seeds can be coated with a toxic chemical by the seed company in order to avoid ingestion. If a package of seeds contain coated seeds this fact shall be stated in the container. Soaking the seeds in hot water for 1/2 hour and Rinsing on a filter should remove this coating. while many varieties of morning glory contain the active LSA (Lysergic acid amide), the yield varies greatly. Therefore, the use Pearly only gates, Wedding Bells, and Sky Blue varieties for The best results.

Reduce the seed material to a fine powder in the blender, and spread it to dry. Grind again if not good enough after the first time due to humidity.

Saturate powdered seed material with lighter fluid, naphtha, or Ligroin.

When completely saturated, it should have the soup consistency. Pour into a chromatographic column and let sit overnight.

Remove the fatty oils from the material by drip to solvent slowly through the column, and testing the liquid that comes through fats by evaporation of a drop in clean glass until it doesn't leave greasy film. (Must have several grams of solvent for each gram of seeds).

Mix 9 volumes of chloroform with 1 volume of concentrate ammonium hydroxide and stirring in a separation funnel. When settling, the chloroform phase will be at the bottom. Drain the chloroform layer and discard the top layer.

Drip the chloroform wash through the column and save the extract. continuously test by evaporation of a drop in cleaning glass until it stops fluorescence.

It is not explicit in the source, but if it is extracted From ergot I would like to start with the alkaloid base of Cravage in this point

The chloroform extracts evaporate, and dissolve the residue in the minimum amount of a 3% solution of tartaric acid. If all the residue does not dissolve, put it in suspension by agitation forcefully.

Colour of the solution with an acid-base indicator, and titre of Find the approximate number of moles of the present alkaloid.

Transfer the solution to a settling funnel, and wash the another ship with acid in order to get all the alkaloids out. Pour the washing liquid into the funnel as well.

Bring the pH to make the solution basic by adding sodium a solution of bicarbonate, and add an equal volume of chloroform.

Shake well, let it resolve, remove the background layer and Book. Again add an equal portion of chloroform, shake, let's solve and remove bottom layer.

Combine chloroform extracts (bottom layer) and it evaporates.

The residue remaining after evaporation is a semi-pure LSA concentrate (lysergic acid amide). Amide requires some experimentation for dosage, but 1 mg of the concentrate It's a reasonable starting point. 1 mg LSA will produce effects comparable to 100 micrograms of LSD.


If there's anything wrong, please correct me, using the translator is bad.
 

HIGGS BOSSON

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You describe a method of extracting LSA from seeds.
It is impossible to obtain LSD in this way.

For the synthesis of LSD, lysergic acid is needed, which can be obtained from ergotamine.
 

LeslieKramer

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Oh! Wow! I had no idea about it. But thanks for sharing. It's interesting to read about all this stuff. But I'm not sure if it's possible to do something like this at home. Still, who knows. Maybe I'll try one day to do something like homemade LSD. Lol! Anyway, I still prefer to have stuff like this made by professionals. Recently, I found out about 1D-LSD, which is basically can be purchased online. I know this stuff from my German friend. But I had a look online and saw that this thing is common in many countries.
 
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beherit

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Very nice bro! Keep it going!
 

Chemical Ali

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Stick to HBW seeds, they are best and more potent for LSA extraction. They do not contain any LSD but can without a doubt serve as a precursor to it. A kilo or two of good seeds can easily yield a few grams of LSD. At 5.000-10.000 doses per gram it's not bad at all actually!

Kind regards,
Ali
 

The-Persian-Fox

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can some one please tell how to synthesis LSD ?
 

HerrHaber

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azides

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Not as claimed in this thread
HerrHaberD-LAME is made into LA using a base hydrolysis to remove the methyl ester.
Basic Hydrolysis of Esters (Saponification)


  • When esters are treated with sodium hydroxide, they are converted into carboxylate salts, which upon neutralization yield carboxylic acids. This process is called basic hydrolysis of esters, or saponification.
  • Hydrolysis occurs via a two step addition-elimination mechanism (nucleophilic acyl substitution)
  • The carboxylic acid is then deprotonated to give a carboxylate.
  • To get the final carboxylic product, acid is added during the workup step.

    HINT it is similar to how MDMA is made from glycidate. An acid work-up restores the carboxylic acid.

    From there you have LA plus any coupling reagent PyBOP and diiethylamine and solvent and your in business


 

HerrHaber

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When dealing with a chiral calboxyl function things are less straight forward, even more so when substrate has two nitrogens as heteroatoms (indole nitrogen is more stable but the quinoline one may be tricky). This is why I make all the fuss until someone claims experimental work, the old-school method with KOH is a classic and I'm hoping for a stereoselective hydrolysis procedure (just because someone claims it doesn't make it experimentally accurate but I'm counting on the fact that those able to write a plausible method flawlessly won't fake the claim). I'm looking forward to start working with this substrate. Cheers!
 
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