UR-144 synthesis from TMCP-indole (large scale). Complete video tutorial.

[HIGGS BOSSON]

Can i use 1-H-Benzolpyrol,Indole-Food grade Kosher(C8H7N)instead of TCMP as main precursor following the above procedure and then obtain the same result?

MrSungImpossible replacement

 

[MrSung]

Good, thanks for your response

 

[hgfhgjkh]

@HIGGS BOSSON , can you tell me what was the final yield in your video? Thanks

 

[WillD]

@HIGGS BOSSON , can you tell me what was the final yield in your video? Thanks

Kaspar HauserYield is written in the article, but for different intermediates will be slightly different.

 

[abbadon]

where i get TMCP-indole ? anyone got already?

 

[Marvin "Popcorn" Sutton]

TMCP-indole is made to order or by yourself. You need to find a chemist who will agree to synthesize it for you, or use the services of a company that does custom syntheses. If you decide to make it yourself, you should contact our Experts. The method of synthesis is written here.

 

[abbadon]

TMCP-indole is made to order or by yourself. You need to find a chemist who will agree to synthesize it for you, or use the services of a company that does custom syntheses. If you decide to make it yourself, you should contact our Experts. The method of synthesis is written here.

Marvin Popcorn Sutton
can you tell me a company which does custom synthesis?
and where i can order the integridents for the TMCP-indole synthesis?
please i need someone tell me trusted sources,
i am completely new in learning working with synthesis.

 

[abbadon]

I am glad that i have found this forum.
Where it was hidden all the time,
that i not know of its existence, until few weeks ago ^^

 

[abbadon]

can you tell me a company which does custom synthesis?
I see indole on the listings page, from china. so, the first step for me is to order that from there, is that correct?

abbadon

 

[abbadon]

and CH2Cl2 from india`? or can i use also Dichloromethane Anhydrous from an european vendor, like nitromethane?

the other integridents i not found yet. SnCl4 and 2,2,3,3-Tetramethylcyclopropanecarbonyl chloride.

 

[abbadon]

and CH2Cl2 from india`? or can i use also Dichloromethane Anhydrous from an european vendor, like nitromethane?

the other integridents i not found yet. SnCl4 and 2,2,3,3-Tetramethylcyclopropanecarbonyl chloride.

abbadonsorry, wrong section. i move to the right place.

 

[aaronstevens]

Does anyone know where I can buy these raw synthetic cannabinoids such as jwh-018 and ur-144

 

[BoonDock]

The video shows a wash at the end using alcohol and a heating up process. The instructions with the pictures do not have this. Whats the best thing to do once you take off the top layer and put it in a mold?

 

[BoonDock]

ur 144

 

[dnkr]

I swear UR-144 was the next best thing after JWH-018.. not crazy strong with risk of detrimental effects but I remember very high quality and smooth research experience

If someone can help me find trusted supplier for main precursor I would greatly appreciate it . i would rather make my own then not know what i'm getting these days

 

[khundongdong]

is this the cas number for the first item?
895152-66-6

 

[WillD]

is this the cas number for the first item?
895152-66-6

khundongdongyes

If someone can help me find trusted supplier for main precursor I would greatly appreciate it . i would rather make my own then not know what i'm getting these days

Write to Zero Day, perhaps he will help.

Whats the best thing to do once you take off the top layer and put it in a mold?

If everything was done correctly, wait until it hardens.

Does anyone know where I can buy these raw synthetic cannabinoids such as jwh-018 and ur-144

For raw materials for synthesis, use listing or write to Zero Day.

 

[dnkr]

7:15-8:00 - filtration of the product on the Büchner funnel, pre-crystallized and cooled alcohol solution. Washing with ice alcohol. Keep in mind that product losses are possible in case of poor crystallization and insufficient cooling.

HIGGS BOSSON
Can you elaborate more on this step? Specifically the "ice alcohol". Does the isopropyl alcohol need to be cooled to a specific temp before pouring to wash? (and does it need to be 99% or would 70% work)?

Also, I'm just curious why the post pictures and your video the top layer to collect with syringe is different colors (the video is dark yellow and yours is more of a dark red? Is that normal? (For my first time synth I don't want to think I messed up if mine turns a completely different color lol)

And I want to thank you very much for the video! I hope we can see more from you for other cannabinoid synths

 

[G.Patton]

Does the isopropyl alcohol need to be cooled to a specific temp before pouring to wash?

dnkrYes, you have to cool it in freezer. In opposite case your product will dissolved partially in warm IPA. Same with 70% IPA. It has to be dry and 99% concentrated.

 

[Zachargi]

Can I replace 1-Bromopentane with 1-bromobutane?