MDMA/Ecstasy-Reinigungsverfahren

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Hallo Freunde, danke für den Beitrag, es funktioniert sehr gut, aber ich habe einen Zweifel, wenn ich kristallisiere (die Kristalle fallen sehr gut aus), erhalte ich keine Kristalle wie die typischen von mdma, es ist etwas ähnliches wie Schneeflocken, wie Eis in einem Glas an einem verschneiten Tag, es ist Glas, aber sehr zerbrechlich. Warum kann ich kein starkes Glas bekommen? Vielen Dank und herzliche Grüße 😊
 

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Hallo, herzlich willkommen! Benutzen Sie einen Kühlschrank für das Kristallisationsverfahren? Je schneller die Abkühlung, desto kleiner die Kristalle.
 
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Ja, natürlich, zuerst lasse ich es stehen, bis es Zimmertemperatur hat, dann sind 15 oder 20 % bereits kristallisiert, dann stelle ich es für 2 Stunden in den Kühlschrank und dann für 3 Stunden in den Gefrierschrank. Fast 100 % des gewaschenen Produkts kristallisiert aus, aber die Kristalle sind sehr zerbrechlich, wenn man sie zum Verpacken anfasst, werden sie zu Sand.
 

Mr Good Cat

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Ich habe IPA ein paar Mal hergestellt, und ich vermute, dass diese "Sand"-Kristallform eine natürliche Eigenschaft der IPA-Kristallisation ist. Versuchen Sie, es in Wasser umzukristallisieren, um große Bergkristalle zu erhalten.
 
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Mr Good Cat

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Mir ist aufgefallen, dass IPA gut geeignet ist, um klebrige schwarze Verbindungen, Nebenprodukte der Synthese, zu entfernen.
 

William Dampier

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Large crystals are obtained with the inclusion of a water molecule. Therefore, sometimes it is better to use aq. HCl acid or add water additionally. You must begin crystallization at room temperature so that the process does not begin quickly. If you show a photo of your crystals, maybe I will tell you that you can change for this and get it in a larger size.
 

Keychainsaw

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I read heat makes it brown in here,
I had some issues with the hobby project. The sirup smelled like methylamine in the glass tray and im afraid there might be some methylamine hcl in the end product. Either way this looks fucked up and it looks like it doesnt want to dry any further. Acetone wash just usually turns it into a black tar. Have to say i forgot to dry it does the 4% aq make a bid difference?

This is what i managed to scrape together and kind of dry out. It tastes more salty than bitter. I dont know how methylamine hcl tastes but drying in the oven doesn't make it appear dryer. Its more tarlike than anything else. I'm ready to give up and just flush it. I did manage to get a whiter one with acetone wash but it has the same non bitter taste. Slightly salty. Could other salts have formed in the process? Maybe the aq layer was pipetted up aswell, in that case it might contain trace amounts of mercury?
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G.Patton

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Have you dried this in an oven? At what temp? I assume, there are not a lot of MDMA in this "product".
Looks looks dog shit.
 

Keychainsaw

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105 Celcius. I did manage to get a few gr of good stuff out it before with acetone washes it yielded only a few gr. Thanks for confirming to toss it than i stop wasting and experimenting on it. To be honest the taste test did not pass and it tasted salty and slightly metallic. It didnt want to dry or crash i will simply dump it. Thanks for the fast reply.
 
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