Método de purificación de MDMA/éxtasis

[K53SK53S]

Hola amigos, gracias por el aporte, funciona muy bien pero tengo una duda, al cristalizar (precipitan muy muy bien los cristales) no consigo cristales como los típicos de mdma, es algo más parecido a copos de nieve, a escarcha de hielo en un vaso en un día de nieve, es cristal pero muy frágil. Por qué no me salen cristales fuertes? Gracias y saludos

 

[G.Patton]

Hola, ¡de nada! ¿Utilizas una nevera para el procedimiento de cristalización? Cuanto más rápido se enfríe, más pequeños serán los cristales.

 

[K53SK53S]

Sí, claro, primero lo dejo fuera hasta que esté a temperatura ambiente, entonces ya ha cristalizado un 15 o 20%, luego lo meto en la nevera durante 2 horas y después en el congelador durante 3 horas. Casi el 100% del producto lavado cristaliza, pero los cristales son muy frágiles, al manipularlos para envasarlos se convierten en arena

 

[Mr Good Cat]

He hecho IPA varias veces, y supongo que este estilo de cristal de "arena" es una propiedad natural de la cristalización del IPA. Intenta recristalizarla en agua para obtener grandes cristales de roca.

 

[K53SK53S]

¿En agua? ¿Cómo se hace así, amigo?

 

[Mr Good Cat]

http://bbzzzsvqcrqtki6umym6itiixfhni37ybtt7mkbjyxn2pgllzxf2qgyd.onion/threads/my-mdma-freebase-crystallization.5069/

 

[Mr Good Cat]

Me he dado cuenta de que el IPA es bueno para eliminar el compuesto negro pegajoso, producto secundario de la síntesis.

 

[William Dampier]

Large crystals are obtained with the inclusion of a water molecule. Therefore, sometimes it is better to use aq. HCl acid or add water additionally. You must begin crystallization at room temperature so that the process does not begin quickly. If you show a photo of your crystals, maybe I will tell you that you can change for this and get it in a larger size.

 

[Keychainsaw]

I read heat makes it brown in here,
I had some issues with the hobby project. The sirup smelled like methylamine in the glass tray and im afraid there might be some methylamine hcl in the end product. Either way this looks fucked up and it looks like it doesnt want to dry any further. Acetone wash just usually turns it into a black tar. Have to say i forgot to dry it does the 4% aq make a bid difference?

This is what i managed to scrape together and kind of dry out. It tastes more salty than bitter. I dont know how methylamine hcl tastes but drying in the oven doesn't make it appear dryer. Its more tarlike than anything else. I'm ready to give up and just flush it. I did manage to get a whiter one with acetone wash but it has the same non bitter taste. Slightly salty. Could other salts have formed in the process? Maybe the aq layer was pipetted up aswell, in that case it might contain trace amounts of mercury?

 

[G.Patton]

Have you dried this in an oven? At what temp? I assume, there are not a lot of MDMA in this "product".
Looks looks dog shit.

 

[Keychainsaw]

105 Celcius. I did manage to get a few gr of good stuff out it before with acetone washes it yielded only a few gr. Thanks for confirming to toss it than i stop wasting and experimenting on it. To be honest the taste test did not pass and it tasted salty and slightly metallic. It didnt want to dry or crash i will simply dump it. Thanks for the fast reply.