JWH-018 süntees. Väikeses mahus.

Bigwest

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Mul on kõik koostisosad, ma üritan jagada 8 & 4 minutit kiirgust 2 poolt 2 minutit ja lasta thé toode jahtus nende vahel, kuid see ei tööta. Kas keegi võiks aidata seda pls.
 

G.Patton

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Võite proovida jagada seda 10-25 sekundi peale. Ärge jahutage neid liiga palju.
 
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Bigwest

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Tere
Ma kontrollisin küll kõiki oma tooraine sulamispunkte. Evry asi selle OK. Kas olete proovinud seda sünteesi koduse mikrolaineahju abil ?

Ma arvan, et see ei tööta. seda saab teha ainult mw-reaktori abil.
 

G.Patton

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Tere, ma ei ole seda teinud. Küsisin selle sünteesi kohta Williamilt. Ty teie tagasiside eest.
 

Bigwest

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Kirjutan Williamile pm. Loodan, et hé vastab. Aga ma olen sûre, et Theres midagi valesti.
 
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Tere. Lihtsalt väike selgitus palve.
Kui kaua me peaksime toote kiiritama, kui kasutame kodust mikrolaineahju---8---4 minutit või 10---25-- sekundit? Ja kas tass peab olema suletud?
 

41Dxflatline

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Kui mikrolained töötavad, siis peaks ka ultraheli töötama
 

Alex7920

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Millist tüüpi mikrolaineahju sobib selle reaktsiooni jaoks? Kas seda reaktsiooni saab teha koduse mikrolaineahjuga?
 

joejoe354354

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Tere,ma tahaksin küsida, kas see meetod on nof sobib masstootmiseks?
 

pakanahesa

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Tere vend, tervitused teile kapten. Selle väike skaala kerge annuse või tugeva annuse jaoks? Thx. Coz ma proovin seda 1. selle ei mõju üldse
 

robloxgelap

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all the ingredients are easily available, but making it looks difficult. is there anyone who can help me? especially for steps 6, 7, and 8 how to filter aluminum oxide, what is the temperature for reflux, and what is the aluminum oxide filtered and then washed for? because in the next step aluminum oxide is not mentioned that it will be used again.
 

soebunies

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@robloxgelap aluminium oksida ga larut dalam etanol, suhu reflux adalah suhu titik didih pelarut, tujuan pencucian aluminium oksida agar bisa digunakan kembali di reaksi berikutnya
 
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robloxgelap

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berarti untuk membuat kembali jwh, ga perlu beli alumunium oksida lagi? dan bisa pake alumunium oksida yang sebelumnya udah pernah dipakai dan sudah di cuci?
 

pakanahesa

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Cek pm bro, anyway ane pake microwave rumahan itu waktu dan suhunya tetap 100 celsius atau waktunya lebih lama bro. Soalnya ga ngefek bro
 

mycelium

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I don't understand people not being able to hear EtOH in the microwave
Or maybe around here everyone has cannabis oil and makes candy and shit.
Microwaves have lights inside.
With 50ml ethanol, I hear it for 15 seconds which is normally enough to make it real warm.
Then short bursts, and looking at the beaker in the microwave.
The slightest bubbles and you stop , because it goes from a couple bubbles to over boiling almost instant.
 

William Dampier

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Yes, you are right. It is often necessary to stop heating, it will be gradual. But there is a solution that looks like this:
P9LmxJuQFb

The condenser is installed through the seal.
 
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