MDMA/ekstazī attīrīšanas metode

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Sveiki, draugi, paldies par ieguldījumu, tas darbojas ļoti labi, bet man ir šaubas, kristalizējoties (kristāli nogulsnējas ļoti labi), es nesaņemu tādus kristālus, kādi raksturīgi mdma, tas ir kaut kas vairāk līdzīgs sniega pārslām, ledus sals glāzē sniegotā dienā, tas ir stikls, bet ļoti trausls. Kāpēc es nevaru iegūt spēcīgu stiklu? Paldies un sveicieni 😊
 

G.Patton

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Sveiki, laipni lūdzam! Vai kristalizācijas procedūrai jūs izmantojat ledusskapi? Jo ātrāka atdzesēšana, jo mazāki kristāli.
 
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Jā, protams, vispirms es to atstāju ārā, līdz tā ir istabas temperatūrā, tad 15 vai 20 % jau ir izkristalizējusies, tad es to ielieku ledusskapī uz 2 stundām un pēc tam uz 3 stundām - saldētavā. Gandrīz 100 % no izmazgātā produkta kristalizējas, bet kristāli ir ļoti trausli, un, kad ar tiem rīkojas, lai iepakotu, tie pārvēršas smiltīs.
 

Mr Good Cat

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Vairākas reizes esmu darījis IPA, un es domāju, ka šis "smilšu" kristalizācijas stils ir dabiska IPA kristalizācijas īpašība. Mēģiniet to pārkristalizēt ūdenī, lai iegūtu lielus akmens kristālus.
 
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Mr Good Cat

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Ko es pamanīju, IPA ir labs, lai noņemtu lipīgo melno savienojumu, sintēzes blakusproduktu.
 

William Dampier

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Large crystals are obtained with the inclusion of a water molecule. Therefore, sometimes it is better to use aq. HCl acid or add water additionally. You must begin crystallization at room temperature so that the process does not begin quickly. If you show a photo of your crystals, maybe I will tell you that you can change for this and get it in a larger size.
 

Keychainsaw

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I read heat makes it brown in here,
I had some issues with the hobby project. The sirup smelled like methylamine in the glass tray and im afraid there might be some methylamine hcl in the end product. Either way this looks fucked up and it looks like it doesnt want to dry any further. Acetone wash just usually turns it into a black tar. Have to say i forgot to dry it does the 4% aq make a bid difference?

This is what i managed to scrape together and kind of dry out. It tastes more salty than bitter. I dont know how methylamine hcl tastes but drying in the oven doesn't make it appear dryer. Its more tarlike than anything else. I'm ready to give up and just flush it. I did manage to get a whiter one with acetone wash but it has the same non bitter taste. Slightly salty. Could other salts have formed in the process? Maybe the aq layer was pipetted up aswell, in that case it might contain trace amounts of mercury?
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G.Patton

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Have you dried this in an oven? At what temp? I assume, there are not a lot of MDMA in this "product".
Looks looks dog shit.
 

Keychainsaw

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105 Celcius. I did manage to get a few gr of good stuff out it before with acetone washes it yielded only a few gr. Thanks for confirming to toss it than i stop wasting and experimenting on it. To be honest the taste test did not pass and it tasted salty and slightly metallic. It didnt want to dry or crash i will simply dump it. Thanks for the fast reply.
 
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