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Benzaldehyde Synthesis

Benzyl Alcohol Oxidation to Benzaldehyde Catalyzed by Acid in DMSO

https://bbgate.com/threads/benzaldehyde-synthesis-from-benzyl-alcohol.611/
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Reactions: The Silent Chemist, smallsky!, psy and 6 others
S
can the dmso, hbr be directly reused in a second run after extraction or does it need to be redistilled and replenished with hbr
 
Johnny_Hammersticks
G.Patton said:
Hi. With toluene as a solvent?
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Hello! Yes I was wondering, but I think I confused this with the oxidization. Toluene can be oxidized to benzaldehyde correct? I think I could get by without some of the equipmemt usef in the video. i.e. reactor, rotoevap and overhead stirrer.
 
G.Patton
Johnny_Hammersticks said:
Hello! Yes I was wondering, but I think I confused this with the oxidization. Toluene can be oxidized to benzaldehyde correct? I think I could get by without some of the equipmemt usef in the video. i.e. reactor, rotoevap and overhead stirrer.
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You can use toluene as a solvent for extraction. You cannot use it for the reaction instead of DMSO.
 
The Silent Chemist
Can you please list all the glass wear and equipment used in this video ?

what is the name of that reaction vessel and its volume? And the size of the rotary still etc

thank you some much, this video is golden
 
Johnny_Hammersticks
You can use toluene as a solvent for extraction. You cannot use it for the reaction instead of DMSO. You sir are awesome and I read through your worms quite a bit on the site. So I don't mean to question your expertise on this subject; but I've found multiple online sources talking about the catalytic oxidization of toluene via concentrated H2O2 at 80⁰c. It seems pretty straightforward and on paper the reaction checks out.
 

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