Amphetamine synthesis from P2NP via Al/Hg (video)

[nitochronic1]

Hello I watch your video and thought it was excellent, but does anyone know where I can order mercury nitrate from and get delivered to the UK ? Thanks

 

[ASheSChem]

you can try to mail reagent-inc (it is not on actual catalogue... but he have a mail..)
or the thermometer tek

 

[nitochronic1]

How can I get hold of them ? Thanks

 

[Mclssmxxl]

Look for a supplier from poland, least restrictive in the EU

 

[cyb3r0]

What is the easy, fast and guaranteed way to get rid of the odor of P2np after synthesis After completion, my washing method is to put the product from Amphetamine in a cup and acetone poured over it until it covered the amphetamine and stirred for about 15 times twice and put in a vacuum bag Is that right?

 

[William Dampier]

Add no more than 20% of water from the total number of solvents at the beginning of the reaction

 

[William Dampier]

The reaction does not pass to the end, there should not be such a smell. What is the color of the product before washing?

 

[cyb3r0]

Yellow

 

[Saul]

I don't think you understand. in sulfuric acid 37% pure there is 63% water in it .
I use the 96 % pure and there is only 4% water in it .
but you can use it this strong becouse it burnt when you add it this pure

 

[ACAB]

And you are using 17gr water to dilute the sulfuric acid to provide burning?
That would be quite strange, normally you salt out in a solvent and dilute the acid with the solvent.

 

[Saul]

just before I need it I mix 17 gr water with 10 gr sulfuric acid 96% and add it verry slowly to my mix off 135ml methanol with 100ml A-oil
I use ice water for cooling .

 

[Marvin "Popcorn" Sutton]

And what's the point of adding water?

 

[Saul]

I have explane it in post #349

greetings

 

[ACAB]

and that is nonesense in my opinion, dillute your acid with methanol if you use it for the oil too. You loose over 17g sulfat with the water. And also i would use a higher amount of solvent for the acid because it is easier to hit the pH 6 point then.

 

[Marvin "Popcorn" Sutton]

Then why add methanol? It will bind your water, and you will not get a water layer. You will get something like a gel that is difficult to separate or filter out. Usually, when acidifying the free base of amphetamine, the dryest ingredients are used to avoid problems with precipitation.
Or you need to do without alcohol so that the salt goes into the aqueous phase and then evaporate the water to obtain salt. By the way, in the case of hydrochloride, this option will not work, only with sulfate.

 

[Toomuchname]

Can I use 85% phosphorus acid instead of sulfuric acid?

 

[ASheSChem]

yes if you want phosphate amphetamine, and not sulfate amphetamine

 

[Toomuchname]

What’s the difference?

 

[ASheSChem]

that's the question
(i have never try phosphate)
information i have read.. officially it's the same...
i have ear phosphate better for IV ? i can't confirm... and best yielding with sulfate ... (but what about purity ?)
and for effect... officially the same but some prefer one, an others no

 

[MadHatter]

Phosphate is somewhat more soluble in water. That's about it. No other interesting differences.