Reningsmetod för MDMA/ecstasy

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Hej vänner, tack för bidraget, det fungerar mycket bra men jag har ett tvivel, när jag kristalliserar (kristaller fälls ut mycket mycket bra) får jag inte kristaller som de typiska för mdma, det är något mer som liknar snöflingor, till isfrost i ett glas på en snöig dag, det är glas men mycket bräckligt. Varför kan jag inte få starkt glas? Tack och hälsningar 😊
 

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Hej, du är välkommen! Använder du ett kylskåp för kristalliseringsproceduren? Ju snabbare nedkylning, desto mindre kristaller.
 
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Ja, naturligtvis, först låter jag den stå framme tills den är rumstempererad, då har 15 eller 20% redan kristalliserat, sedan lägger jag den i kylskåpet i 2 timmar och sedan i frysen i 3 timmar. Nästan 100% av den tvättade produkten kristalliserar, men kristallerna är mycket ömtåliga, när de hanteras för förpackning förvandlas de till sand
 

Mr Good Cat

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Jag gjorde IPA några gånger, och jag antar att denna "sand" kristallstil är en naturlig egenskap hos IPA-kristallisering. Försök att omkristallisera den i vatten för att få stora bergkristaller.
 
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Mr Good Cat

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Vad jag märkte, IPA är bra för att ta bort klibbig svart förening, biprodukt av synth.
 

William Dampier

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Large crystals are obtained with the inclusion of a water molecule. Therefore, sometimes it is better to use aq. HCl acid or add water additionally. You must begin crystallization at room temperature so that the process does not begin quickly. If you show a photo of your crystals, maybe I will tell you that you can change for this and get it in a larger size.
 

Keychainsaw

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I read heat makes it brown in here,
I had some issues with the hobby project. The sirup smelled like methylamine in the glass tray and im afraid there might be some methylamine hcl in the end product. Either way this looks fucked up and it looks like it doesnt want to dry any further. Acetone wash just usually turns it into a black tar. Have to say i forgot to dry it does the 4% aq make a bid difference?

This is what i managed to scrape together and kind of dry out. It tastes more salty than bitter. I dont know how methylamine hcl tastes but drying in the oven doesn't make it appear dryer. Its more tarlike than anything else. I'm ready to give up and just flush it. I did manage to get a whiter one with acetone wash but it has the same non bitter taste. Slightly salty. Could other salts have formed in the process? Maybe the aq layer was pipetted up aswell, in that case it might contain trace amounts of mercury?
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G.Patton

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Have you dried this in an oven? At what temp? I assume, there are not a lot of MDMA in this "product".
Looks looks dog shit.
 

Keychainsaw

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105 Celcius. I did manage to get a few gr of good stuff out it before with acetone washes it yielded only a few gr. Thanks for confirming to toss it than i stop wasting and experimenting on it. To be honest the taste test did not pass and it tasted salty and slightly metallic. It didnt want to dry or crash i will simply dump it. Thanks for the fast reply.
 
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