Metamfetamin från efedrin med hjälp av jod och röd P

hacke8

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Förlåt, jag skickade det flera gånger.
 

TheNut22

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Kan jag använda bara KI-kristaller förutom jodonkristallerna i den här syntesen, vet du det? Jag kan extrahera jod från den KI men vad jag har läst ...
 

Anarchy Labz

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Varför använde du dcm, kan detta göras utan dcm? Är det inte också lite mycket att använda 12 g I2 för 6 g efedrin?
 

GhostChemist

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Du kan använda petroleumeter, bensen eller toluen
 

Bmth

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Vilken är den bästa av alla sjömän i Vilken av dessa typer av sjömän är bäst i mitt land är svårt att hitta
Indonesiska:
 

TheNut22

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Kan jag använda xylen i stället för DCM?
 

handle

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I vilket skede skulle det genereras fosgen?
 

hacke8

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Den kommer inte att producera fosgen. Det kommer att finnas vätefosfidgas om det är mer än 130. Var försiktig med detta.
 
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TheNut22

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Japp! :). När jag gör denna syntes, om jag lägger PVC-slang från kondensor till en gasfälla full av natriumkarbonat och aktivt kol, vad kan jag göra för att förhindra att gasfällans vattenlösning suger tillbaka till min reaktionsflaska? Har du gett idéer, handtag?
 

rampage

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use a condom ontop of condenser
 

bigclit

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Kan någon länka mig till en one pot-metod där jag kan få allt material personligen. Idc om jag bara hamnar med lite smutsig meth som bara letar efter ett projekt medan fru är ute ur stan för helgen.
 

Hypnou

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Duuuude snälla du gör inte det, finns verkligen många bättre metoder vad du kan lära dig själv, bara för respekt för matlagning 🫠
 

iceberg

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Hur många ml ska glasballongen vara och hur stor ska återflödeskondensorn vara? Kan du vara snäll och svara?
 

G.Patton

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Vilken ballong pratar du om? Standard Allihn återflödeskondensor, medelstor.
 

iceberg

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Det finns NH4Cl och H2SO4 i listan. Var exakt används dessa i syntes? Tack för svaret.
 

micked24

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Ammonium Chloride and Sulfuric Acid are combined to produce Hydrogen Chloride. Which is a gas that is used to turn the freebase into a hydrochloride salt. It is used towards the end of the video.
 

TheNut22

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Kan jag använda xylen i stället för DCM?
 

TheNut22

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Jag tror att jag kan det.
 

GhostChemist

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if o-xylene this is bad idea (B.P. 144C)
better petroleum ether, diethyl ether, benzene, toluene etc.
 

Pinkbay

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Om jag tillsätter vatten och hcl för att surgöra den fria basen när jag gör en fri bas, separerar vattenskiktet och avdunstar vattnet helt, kommer salt att dyka upp i slutändan? I teorin behövs inte väteklorid?
 

GhostChemist

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When the free base extracted with DCM, you can use aqueous HCl for obtain salt after evaporation
 

rampage

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can phenylpropanolamine be used instead of ephedrine in this synth?
 

William D.

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Yes. If you have a supplier, send me a DM. The only problem is that the yield may be less than with the methylated version.
 

Chemtrail

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Seen that chemical on an Asian (India) chemical company for good price

Think that chemical is being used as an animal dog medicine
 

Chemtrail

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Swim had done this "red, white, blue" process with 6g E, 6g I, 3 g Rp and a couple of mls of D-H20 in a heat proof Corona beer glass bottle as a RXN vessel, a rubber stopper with airleak-proof connection with 5 foot tubing vertical and a punch balloon as a condenser, used a portable rice cooker & sand bath as heat source ~100-120C for 24 hours

Long Wet Reaction

Off heat to cool. Add 100 ml D-H20 . Filter Rp (**WASH OUT THE RP WITH HOT ACID, HOT ALCOHOL, HOT ACETONE, lukewarm water** good as new)
Add NaOH base solution till pH 12 A WHITE SLURRY WILL APPEAR
Extract with a NP fuel several times
Wash NP fuel/chilli with baking soda solution and then a D-H20 wash
Dry with drying agent for minutes and filter

Get a shot glass of D-H20 and drop 2-3 drops of HCl (or sulfuric acid) in it. Put this shot glass water with the NP/chilli and shake

Repeat several times

Extract water/chilli and evaporate on LOW heat

Speed a few hundred milligrams but good



* Swim got a VERY small percent yeild doing this method :(

Why did swim with 6 G of pseudoephedrine ended up with just a few hundred milligrams of speed ?! :(
 

Chemdog010297

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Can we get a synthesis of two for propiophenone ?
 

Chemtrail

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Think you can make synthetic Ephedrine from propiophenone, there is a video

And don't seem very complicated
 

Chemdog010297

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Can I do this synthesis at 140 Fahrenheit for 48 hours and get the same result ?
 
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