4-MMC synthesis

MMX

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ngl thats a "wow" result :D
 

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ngl thats a "wow" result :D
MMXBut crystallization takes too long, needed finished product sooner so the rest batches I rapid crystallized. Maybe when BK4 arrives I do couple batches like this
 
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But crystallization takes too long, needed finished product sooner so the rest batches I rapid crystallized. Maybe when BK4 arrives I do couple batches like this
Berlin777I was collecting eq for last month and im omw to do a 1st batch, i hope it will result in such purity outcome, would be a december dream
 

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I was collecting eq for last month and im omw to do a 1st batch, i hope it will result in such purity outcome, would be a december dream
MMXI still have some dirty shit to clean up with acetone after the batches I fucked up
 

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I still have some dirty shit to clean up with acetone after the batches I fucked up
Berlin777thats fascinating that chemistry lets you clean a fucked up job, but like in every industry probably its better to not fuck it up 1st time. I cant wait out for my 1st outcome
 

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I still have some dirty shit to clean up with acetone after the batches I fucked up
Berlin777was 6l roundbottom flask helpful? or would you take bigger one. I ve got 3 necked round 2l, separators 1l and im thinking if its gonna be to be helpful to have 6l roundbottom, they are pretty cheap anyways
 

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thats fascinating that chemistry lets you clean a fucked up job, but like in every industry probably its better to not fuck it up 1st time. I cant wait out for my 1st outcome
MMXThat’s why the batches wasn’t too significant, fuck up was taken under consideration
 

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was 6l roundbottom flask helpful? or would you take bigger one. I ve got 3 necked round 2l, separators 1l and im thinking if its gonna be to be helpful to have 6l roundbottom, they are pretty cheap anyways
MMXI would definitely get bigger separator
The size of the flask depends on the batch you gonna cook. You can start with this small one but if you’re planning batches bigger than 500g even the 6L is too small.

For 100g BK4 I used 1L flask
500g 6L flask
Got 20L flask ready but I’m waiting for the stirring rod
 

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That’s why the batches wasn’t too significant, fuck up was taken under consideration
Berlin777I dont think i understood clearly, did you mean that it was too small floask or just that its not a correct equipment? But finally you received "wow" anywaYS
 

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That’s why the batches wasn’t too significant, fuck up was taken under consideration
Berlin777I have 2 l 3 neck flask, some condensers from used eq i bought, many small flasks etc under 1l, but from eq i bought for 1st synthesis except that flask i already have vacuum pump and buchners funnel 1l fi 125 and separators for 1l, equipment prepared for 100 g batches
 

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I dont think i understood clearly, did you mean that it was too small floask or just that its not a correct equipment? But finally you received "wow" anywaYS
MMXIf you have some spare funds I would get 2L separator instead of 1L. I struggled with 2L due to volume I had to handle. But it all depends on the BK4 batch you planning to cook
 

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If you have some spare funds I would get 2L separator instead of 1L. I struggled with 2L due to volume I had to handle. But it all depends on the BK4 batch you planning to cook
Berlin777I ve watched Marvin's 100g method and bought eq for that.
I have 2 or 3 separators, i bouyght for "almost free" a box with labo glassware there is many separators 500ml - 1l, lots of flask etc, so probably can work with all of them
 

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I have 2 l 3 neck flask, some condensers from used eq i bought, many small flasks etc under 1l, but from eq i bought for 1st synthesis except that flask i already have vacuum pump and buchners funnel 1l fi 125 and separators for 1l, equipment prepared for 100 g batches
MMXI haven't used any condenser yet but I know they're gonna be needed for other synthesis. Flasks under 1L are useless I would say.
But yeah to start with small volumes and learn how to handle BK4, how to wash etc it's ok. Have you already opened your BK4? Got any decent respirator mask?
 

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I haven't used any condenser yet but I know they're gonna be needed for other synthesis. Flasks under 1L are useless I would say.
But yeah to start with small volumes and learn how to handle BK4, how to wash etc it's ok. Have you already opened your BK4? Got any decent respirator mask?
Berlin777I dont have any regeants yet, some of my eq arrives this week. I have some respirator mask but its probnably not for chenmical use, it was a2 p3 or something like that, for painting
probably gonna still need to investigate in that way. I planned to do everything with a hands, month ago i bought eq then i was reading a forum about everything
 

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I dont have any regeants yet, some of my eq arrives this week. I have some respirator mask but its probnably not for chenmical use, it was a2 p3 or something like that, for painting
probably gonna still need to investigate in that way. I planned to do everything with a hands, month ago i bought eq then i was reading a forum about everything
MMX i was inspired as hell on that. when i was 11 or so i loved chemistry but i left that way cuz i was scared it will finish to doing drugs, yet its more than 10 years later still I will do it
 

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I dont have any regeants yet, some of my eq arrives this week. I have some respirator mask but its probnably not for chenmical use, it was a2 p3 or something like that, for painting
probably gonna still need to investigate in that way. I planned to do everything with a hands, month ago i bought eq then i was reading a forum about everything
MMXIt's better to be equipped with aspirator mask handling bk4, once you open it you're gonna see what I mean. You got MA40% or MA HCl?
 

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i was inspired as hell on that. when i was 11 or so i loved chemistry but i left that way cuz i was scared it will finish to doing drugs, yet its more than 10 years later still I will do it
MMXTo start with it's all good but I don't think you're gonna spend several days cooking 100g bk4 batches. The experts probably gonna tell you more because I just started and got only few weeks experience. Bear in mind there will be a lot of smell and even your clothes will smell of mephedrone
 

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To start with it's all good but I don't think you're gonna spend several days cooking 100g bk4 batches. The experts probably gonna tell you more because I just started and got only few weeks experience. Bear in mind there will be a lot of smell and even your clothes will smell of mephedrone
Berlin777oh I see, smell probably is a bad thing but in Marvin's tutorial he uess sodium biocarbonate to exhaust fumesfrom flask, i was thinking to use one time clothing as well. i have some fans and some carbon filters, but not sure if they will work

i dont have any ingridients yet, just only eq, but i ve found that promotion post so I am already in cotact with William
 

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To start with it's all good but I don't think you're gonna spend several days cooking 100g bk4 batches. The experts probably gonna tell you more because I just started and got only few weeks experience. Bear in mind there will be a lot of smell and even your clothes will smell of mephedrone
Berlin777probably will use 40% aq MA
 

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To start with it's all good but I don't think you're gonna spend several days cooking 100g bk4 batches. The experts probably gonna tell you more because I just started and got only few weeks experience. Bear in mind there will be a lot of smell and even your clothes will smell of mephedrone
Berlin777do you know what parametres a mask should have ? probably it will be some signs or something, i ve serached on my hand but didnt get a lot of info. I dont know if "anti gas" is enough
 

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3m 6057 are filters model for my maks, is it suitable for that? its called in description thats to work with gases of 0.1 (1000ppm) in air
MMXI do have 3M as well but I’m unsure what model, gonna take a look tomorrow but I know it’s great. If you’re buying 3M I recommend also buying spare harness. Mine just snapped recently in the middle of synthesis when I was putting my mask on
 

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I do have 3M as well but I’m unsure what model, gonna take a look tomorrow but I know it’s great. If you’re buying 3M I recommend also buying spare harness. Mine just snapped recently in the middle of synthesis when I was putting my mask on
Berlin777oh sorry i went out of reply,


I alrteady have 3m mask beacsue earlier i needed it for somethin else, but filters are outdated for such thing ,i found that 6099 is the best, there is even MA described, clorides etc. I dont have full maks but i have gloves for eyes with protective gum


can you link that wet filtration, i mean i typed into search but cant see a topic
 
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