4-MMC synthesis

[cascade]

N.m.p n methyl pyroldin
Not an expert but after successful failures came to know that if we add nmp water and ethyl acetate should be done above 55°...ethyl acetate boiling 70 above but as suggested in video 60°, adding EA at that time colour becomes dark red saturated...
But if we so with dcm i did not get that problem colour of organic layer is golden yellow as shown in video.
Even precipitation got faster while adding hcl itself got precipitation
You Can notice it in below pics

cherryindiabecause u dont wash freebase and get dark color

 

[🍒cherry]

N.m.p n methyl pyroldin
Not an expert but after successful failures came to know that if we add nmp water and ethyl acetate should be done above 55°...ethyl acetate boiling 70 above but as suggested in video 60°, adding EA at that time colour becomes dark red saturated...
But if we so with dcm i did not get that problem colour of organic layer is golden yellow as shown in video.
Even precipitation got faster while adding hcl itself got precipitation
You Can notice it in below pics

cherryindiabecause u dont wash freebase and get dark color

 

[BitcoinScam]

N.m.p n methyl pyroldin
Not an expert but after successful failures came to know that if we add nmp water and ethyl acetate should be done above 55°...ethyl acetate boiling 70 above but as suggested in video 60°, adding EA at that time colour becomes dark red saturated...
But if we so with dcm i did not get that problem colour of organic layer is golden yellow as shown in video.
Even precipitation got faster while adding hcl itself got precipitation
You Can notice it in below pics

cherryindiabecause u dont wash freebase and get dark color

 

[BitcoinScam]

cold way is shit way because your product no get euphoria dcm u need only heat.
dmso nmp THF u dont need u can do like u say now.
i never no made m40% form M HCL.
M40% i buy for 14€/L but if thet ban good to know how to made m40% form M hcl

 

[Marvin "Popcorn" Sutton]

cold way is shit way because your product no get euphoria dcm u need only heat.
dmso nmp THF u dont need u can do like u say now.
i never no made m40% form M HCL.
M40% i buy for 14€/L but if thet ban good to know how to made m40% form M hcl

BitcoinThere is no way heating affects euphoricity, only reaction time. Don't be misled.
If the reaction is done correctly, you will not be able to tell from the quality of the product the method used to produce it.
This topic is about the method used by Berlin777 .
You can post your personal syntheses separately in a suitable topic.

 

[BitcoinScam]

There is no way heating affects euphoricity, only reaction time. Don't be misled.
If the reaction is done correctly, you will not be able to tell from the quality of the product the method used to produce it.
This topic is about the method used by Berlin777 .
You can post your personal syntheses separately in a suitable topic.

Marvin "Popcorn" Suttoneach solvent has its own time and temperature for the reaction to occur correctly dcm 2h 40°c toulene 60°c 2h dsmo 20min mix nmp 30nin mix There is a Russian table circulating on the Internet with charts and what temperature and time should be For 2bromo4methylenepropiophenone and for 2iodo4methylenepropiophenone. from what I noticed in this synthesis and written in others very well and the same applies to bk mdma 3mmc 3cmc 4cmc 4mmc 2mmc free base washing water water and soda extraction and then souring if the soluble is not miscible with water, e.g. dcm toulen, you can use water to select 4mmc, add ipa/ethylene acetate l/acetone and crystallize it without filtering the powder. or play around and use acetone and filter the powder and then crystallize. This is the production philosophy 4mmc 3mmc 3cmc 4cmc bk mdma 2mmc 3cec 4cec apvp

 

[🍒cherry]

each solvent has its own time and temperature for the reaction to occur correctly dcm 2h 40°c toulene 60°c 2h dsmo 20min mix nmp 30nin mix There is a Russian table circulating on the Internet with charts and what temperature and time should be For 2bromo4methylenepropiophenone and for 2iodo4methylenepropiophenone. from what I noticed in this synthesis and written in others very well and the same applies to bk mdma 3mmc 3cmc 4cmc 4mmc 2mmc free base washing water water and soda extraction and then souring if the soluble is not miscible with water, e.g. dcm toulen, you can use water to select 4mmc, add ipa/ethylene acetate l/acetone and crystallize it without filtering the powder. or play around and use acetone and filter the powder and then crystallize. This is the production philosophy 4mmc 3mmc 3cmc 4cmc bk mdma 2mmc 3cec 4cec apvp

BitcoinBk mdma? Can we do mdma with bk? Can u share the process if available

 

[BitcoinScam]

Bk mdma? Can we do mdma with bk? Can u share the process if available

cherryindiau cant made form bk mdma to mdma if u want made mdma u need Piperonal and later mdp2p or use pmk glicydate if u want made mda u can use Piperonal mdp2p or helional

 

[Berlin777]

Yeah the first ones looked very dirty, I only showed them to compare to current ones, which are cleaner, I am aware of mistakes which I’m trying to fix, ordering few things to improve production and quality.

If you can safely ship MA40% to the UK I will be happy to buy it.

 

[Berlin777]

It’s cleaner compared to my first batches

 

[BitcoinScam]

It’s cleaner compared to my first batches

Berlin777can u send more picture how to look freebase when and how too looks like 2b4m in dcm when u throw naoh water and later m hcl?

 

[Berlin777]

can u send more picture how to look freebase when and how too looks like 2b4m in dcm when u throw naoh water and later m hcl?

BitcoinI usually don't save such pictures on my phone. Only sometimes take a picture to send it and delete it right away. I do have only one 2L separation funnel, do you think that would work to use hose and vacuum to pump out the layer from the flask?

 

[Marvin "Popcorn" Sutton]

Please post your synthesis reports in separate threads and discuss them there. This thread was created for an example of a synthesis that Berlin777 made.
Berlin777 has made a great 4mmc, we made sure of it.

 

[🍒cherry]

Please post your synthesis reports in separate threads and discuss them there. This thread was created for an example of a synthesis that Berlin777 made.
Berlin777 has made a great 4mmc, we made sure of it.

Marvin "Popcorn" SuttonThanks 2 @Berlin and g.patto

 

[Berlin777]

How it’s going

 

[🍒cherry]

How it’s going

Berlin777Nice,

 

[🍒cherry]

Nice,

cherryindiaOne again 2 @William Dampier @Berlin777 @G.Patton

 

[G.Patton]

One again 2 @William Dampier @Berlin777 @G.Patton

cherryindiaCongratulations! Can you please make a new topic and describe in details your synthesis please? We will be appreciated for that!

 

[🍒cherry]

Congratulations! Can you please make a new topic and describe in details your synthesis please? We will be appreciated for that!

G.PattonWill do thank you for your help patton some instructions and error checks from you helped me alot ....

 

[G.Patton]

Will do thank you for your help patton some instructions and error checks from you helped me alot ....

cherryindiaYou are welcome

 

[Berlin777]

I think customers gonna love this size of crystals, now the only things is to keep this up.
I personally preferred fine size of crystals as it’s much easier to sniff but I know people gonna be attracted by bigger ones

 

[dragonballScam]

how much gram crystal u get form 100g 2b4m ?

dragonballI haven’t weighted yet, had to pick them for someone before it all fully crystallised

I was roughly getting 50-60% powder

 

[Berlin777]

how much gram crystal u get form 100g 2b4m ?

dragonballI haven’t weighted yet, had to pick them for someone before it all fully crystallised

I was roughly getting 50-60% powder

 

[Berlin777]

when i throw all methyloamine too jar and u mix how color freebase have ?

dragonball@dragonball it’s all as it should be, if you’re such a specialist why don’t you share your method?

 

[Aaron]

Thank you for your insights, Berlin777.
It will help other people with the similar issues.

 

[MMX]

ngl thats a "wow" result

 

[Berlin777]

ngl thats a "wow" result

MMXBut crystallization takes too long, needed finished product sooner so the rest batches I rapid crystallized. Maybe when BK4 arrives I do couple batches like this

 

[Berlin777]

3m 6057 are filters model for my maks, is it suitable for that? its called in description thats to work with gases of 0.1 (1000ppm) in air

MMXI do have 3M as well but I’m unsure what model, gonna take a look tomorrow but I know it’s great. If you’re buying 3M I recommend also buying spare harness. Mine just snapped recently in the middle of synthesis when I was putting my mask on

 

[MMX]

I do have 3M as well but I’m unsure what model, gonna take a look tomorrow but I know it’s great. If you’re buying 3M I recommend also buying spare harness. Mine just snapped recently in the middle of synthesis when I was putting my mask on

Berlin777oh sorry i went out of reply,


I alrteady have 3m mask beacsue earlier i needed it for somethin else, but filters are outdated for such thing ,i found that 6099 is the best, there is even MA described, clorides etc. I dont have full maks but i have gloves for eyes with protective gum


can you link that wet filtration, i mean i typed into search but cant see a topic