4MMC/MEC large crystals

Sergey Kush

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4-MMC in dry methanol. T 15-20C, 1 week
 

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Netflix

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Only water is no posible with only water get like this crystal
 

Sergey Kush

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IPA for crystallization 4-mmc is bad. Methanol is the best
 

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Im made with ipa and made like you see you made 3 week because you use to much water simple
 

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In acetone you can do ipa pure wodka from shop is much ways
 

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How you guys clean the freebase? Only water or NaOH also or Sodium Bisulfite solution?
How long you cook the DCM with 2b4m and at what temperature?
 

Sergey Kush

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How you guys clean the freebase? Only water or NaOH also or Sodium Bisulfite solution?
How long you cook the DCM with 2b4m and at what temperature?
ChingShihafter the reaction of 2b4m with methylamine in DCM, the free base of mephedrone is washed 2-3 times with an equal volume of water. the reaction with methylamine lasts 4 hours at a temperature of 32-36C. do not bring DXM to a boil (38C), as DHM hydrolyzes when boiling, the free base will be heavily contaminated. if the temperature/time is observed, the free base will be very clean.
 
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