Dextroamphetamine Synthesis (Nabenhauer, 1942)
- Thread starter G.Patton
- Start date
As for MDA synth, I hate to disappoint but I bought the md-p2np already made - I don’t like the group of drugs enough to bother doing the Henry reaction etc but seeing as I saw it for sale, I reduced some over the previous couple days (via NaBH4 catalysed by copper - although from my understanding there are many ways to reduce nitroalkene’s) and now I have a bunch of r-MDA.
Now I will follow the latter part of the synthesis from where you have your r-amphetamine.
I can’t say I have ever seen 3,4-MDbenzaldehyde for sale…I take it that is the same as piperonal?
Now I will follow the latter part of the synthesis from where you have your r-amphetamine.
I can’t say I have ever seen 3,4-MDbenzaldehyde for sale…I take it that is the same as piperonal?
hey patton !
i HATE Hg-Salts......
(who doesnt ?) I MANAGED TO SUBSTITUTE THE AGENT; to break the oxide layer, by catalyst poisoning,
YOU CAN USE SEVERAL OTHERS LIKE:
1. Gallinstan (known in newer lit. already, but a bit trickyer...)
2. Tetrachloroaurate with zinc-copper coupling complex.
===== BUT NOW, LADIES AND GERMS ============
PRE TREAT THE ALUMINUM CUTTINGS WITH ULTRA SONICATION BATH
(CREDITS TO ARTIFFICCIAL INTELLIGENCE FOR SCIENTIFIC PURPOSES)
this f**king DID THE JOB !!!!!
tried it for p2p -> imine reduction......its comparable to my former NaBH4 dreams...!
i HATE Hg-Salts......
(who doesnt ?) I MANAGED TO SUBSTITUTE THE AGENT; to break the oxide layer, by catalyst poisoning,
YOU CAN USE SEVERAL OTHERS LIKE:
1. Gallinstan (known in newer lit. already, but a bit trickyer...)
2. Tetrachloroaurate with zinc-copper coupling complex.
===== BUT NOW, LADIES AND GERMS ============
PRE TREAT THE ALUMINUM CUTTINGS WITH ULTRA SONICATION BATH
(CREDITS TO ARTIFFICCIAL INTELLIGENCE FOR SCIENTIFIC PURPOSES)
this f**king DID THE JOB !!!!!
tried it for p2p -> imine reduction......its comparable to my former NaBH4 dreams...!