FAILED REACTION 2-IODO-4MP

[INDIANELK]

I TRIED MY MAKING 2-IODO-4MP FIRST TIME EXACTLY AS THE GIVEN RECEPIE IN THE VEDIO ON FORUM IT STARTED OUT AS EXPECTED I ADDING ALL INGREDIENTS AS MENTIONED I GOT SAME LOOKING RM PITCH RED BLACK BROWN BUT WHEN I LEFT IT AND CAME AFTER 6 HOURS THE COLOURS WAS CHANGED TO LIGHT BROWN LIKE COFFEE HOW DID IT HAPPEN CAN SOMEBODY HELP I BOUGHT THE REAGENTS FOR VERY HEFTY PRICE FOR THE FIRST TRY AND IT FAILED CAN SOMEBODY TELL WHY I AM ATTACHING A PHOTO THE IODONE COLOUR IS GONE @Novator @G.Patton pls help experts

 

[G.Patton]

First of all, hello. Please, do not type in Caps Lock. We can read lower case letters. It's not so nice.

Do you mean this video?

Download Video

Mephedrone synthesis

• Novator
• Apr 6, 2023
• 79
• 2-iodo-1-p-tolyl-propan-1-one 2-iodo-4'-methylpropiophenone 4-mmc cas 236117-38-7 meph mephedrone mephedrone hydrobromide mephedrone hydrochloride mephedrone video synthesis

Mephedrone synthesis from 2-iodo-4'-methylpropiophenone (CAS 236117-38-7) with ethyl acetate...

BUT WHEN I LEFT IT AND CAME AFTER 6 HOURS THE COLOURS WAS CHANGED TO LIGHT BROWN LIKE COFFEE HOW DID IT HAPPEN

Have you left mephedrone free base in open vessel for 6 hours? Am I right?

 

[INDIANELK]

First of all, hello. Please, do not type in Caps Lock. We can read lower case letters. It's not so nice.

Do you mean this video?

Download Video

Mephedrone synthesis

• Novator
• Apr 6, 2023
• 79
• 2-iodo-1-p-tolyl-propan-1-one 2-iodo-4'-methylpropiophenone 4-mmc cas 236117-38-7 meph mephedrone mephedrone hydrobromide mephedrone hydrochloride mephedrone video synthesis

Mephedrone synthesis from 2-iodo-4'-methylpropiophenone (CAS 236117-38-7) with ethyl acetate...

Have you left mephedrone free base in open vessel for 6 hours? Am I right?

G.PattonNo @G.Patton I mean the 2-iodo-4 methylepropiophenone vedio

 

[G.Patton]

No @G.Patton I mean the 2-iodo-4 methylepropiophenone vedio

INDIANELKCan you be more specific in your problem description please? Describe your step-by-step procedure and all reagent amounts.

 

[INDIANELK]

 

[INDIANELK]

View attachment 22483

INDIANELK@G.Patton so I followed this VEDIO step by step first added 4mp as given quantity second added ipa as given third added cup as given and after that I added iodine as given everything was looking right as in the VEDIO then I left it for stirring at 60-65 degrees as mentioned and when I came back to check after 6 hours the colour of RM changed to brown unlike the reddish brown black in the VEDIO why so as of now 17+ hours of stirring is completed and I removed the RM in vessel cup was there in the flask but the colour is brown not reddish like in the VEDIO

 

[G.Patton]

Can you apply pictures of your reaction mixture?

step by step first added 4mp as given quantity second added ipa as given third added cup as given and after that I added iodine as given everything was looking right as in the VEDIO

Have you added CuO as said in tutorial?

IT AND CAME AFTER 6 HOURS THE COLOURS WAS CHANGED TO LIGHT BROWN LIKE COFFEE

If you read this tutorial, you should know that you have to heat and stir reaction mixture not less than 15h (not 6).

The reaction mixture is heated to 70 °C, then reaction is left for 24 h with a constant stirring and heating.

Have you got such suspension in your reaction mixture?

P.S. If you punctuate your text, it will be much easier and convenient to read.

 

[INDIANELK]

Can you apply pictures of your reaction mixture?

Have you added CuO as said in tutorial?

If you read this tutorial, you should know that you have to heat and stir reaction mixture not less than 15h (not 6).


Have you got such suspension in your reaction mixture?
View attachment 22548

P.S. If you punctuate your text, it will be much easier and convenient to read.

G.PattonNo I didn't look like this ..I know I have to heat and stir for 15 hrs and also I did stir it for 17+ hours but what I was saying is in the start when I started everything the Rm looked same as in VEDIO but after 6 hours passed when I came to check the colour of RM bacame light brown unlike in the VEDIO also after 17+ hours the mixture didn't look like the one in VEDIO

 

[G.Patton]

No I didn't look like this ..I know I have to heat and stir for 15 hrs and also I did stir it for 17+ hours but what I was saying is in the start when I started everything the Rm looked same as in VEDIO but after 6 hours passed when I came to check the colour of RM bacame light brown unlike in the VEDIO also after 17+ hours the mixture didn't look like the one in VEDIO

INDIANELKYou didn't answer my questions

 

[INDIANELK]

You didn't answer my questions

G.PattonWhich question

 

[INDIANELK]

You didn't answer my questions

G.PattonNo I didn't get the same looking suspension it became light brown

 

[G.Patton]

Which question

INDIANELK

Have you added CuO as said in tutorial?

 

[G.Patton]

No I didn't look like this ..I know I have to heat and stir for 15 hrs and also I did stir it for 17+ hours but what I was saying is in the start when I started everything the Rm looked same as in VEDIO but after 6 hours passed when I came to check the colour of RM bacame light brown unlike in the VEDIO also after 17+ hours the mixture didn't look like the one in VEDIO

INDIANELKHave you heated your reaction during this 17 hours or no?

 

[INDIANELK2]

Have you heated your reaction during this 17 hours or no?

G.PattonYes I did everything exactly as shown

 

[G.Patton]

Yes I did everything exactly as shown

INDIANELK2If you did everything like in the video, probably a problem is in your reagents. What CAS of 4mp did you use? Are you sure that it was 4'-methylpropiophenone?

 

[INDIANELK2]

If you did everything like in the video, probably a problem is in your reagents. What CAS of 4mp did you use? Are you sure that it was 4'-methylpropiophenone?

G.Patton@G.Patton exactly I was thinking the same I acquires two samples from two different local vendors one was dark yellow other was pure white. The white one smelled very good the yellow one was bitter smelling I tried that with the yellow one first and the reaction failed and now I am trying with the white one letss see what happens . As far as I know the reaction not so hard to perform right. I also tried with hbr on the yellow one when I added hydrogen peroxide it turned red then yellow but after follow exactly same method as shown in vedio it still didn't percipitate even after 24 hours of stirring

 

[G.Patton]

@G.Patton exactly I was thinking the same I acquires two samples from two different local vendors one was dark yellow other was pure white. The white one smelled very good the yellow one was bitter smelling I tried that with the yellow one first and the reaction failed and now I am trying with the white one letss see what happens . As far as I know the reaction not so hard to perform right. I also tried with hbr on the yellow one when I added hydrogen peroxide it turned red then yellow but after follow exactly same method as shown in vedio it still didn't percipitate even after 24 hours of stirring

INDIANELK2You shouldn't try your reagent's taste. It won't help you determine its quality, just poison you and help to get cancer. Check its melting point, man. Easy method to check.

 

[INDIANELK]

You shouldn't try your reagent's taste. It won't help you determine its quality, just poison you and help to get cancer. Check its melting point, man. Easy method to check.

G.Patton@G.Patton how can I pm you I want some guidance man tried it again and seems like I am failing miserably I'll pay you if you want pls help me out

 

[xoxoxoxo]

2i4m can be made in a microwave, which is not as expensive as it is, much faster

 

[INDIANELK2]

2i4m can be made in a microwave, which is not as expensive as it is, much faster

xoxoxoxoCan you tell how

 

[INDIANELK2]

2i4m can be made in a microwave, which is not as expensive as it is, much faster

xoxoxoxoIn an easy way so i can understand

 

[INDIANELK2]

2i4m can be made in a microwave, which is not as expensive as it is, much faster

xoxoxoxoI'll be very thankful to you