MDMA synthesis via NaBH4 from MDP2P

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Sir i would like to know after finish add nabh4. Is room temperature stir 12 hour or what? After 12 hour add water and hci is room temperature add or how?
 

G.Patton

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It isn't said that you need keep low temperature. Hence, you can stir it at room temperature.
>>> The mixture is stirred for 2 days.

>>>After 12 hour add water and hci is room temperature add or how?
You need to avoid overheating and cool the mixture temperature down in case of temperature rising more than 40-50*C.
 

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Noted with thanks. I know how to do. Any result i will let you know
 

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Why does the powder appear after I rotate the distillation? Didn't you get the oily material and then put in the hydrochloric acid gas?
 

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Please, write me clearly in DM. You have flooded the topic by questions.
 
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