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G.Patton

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SonicNL

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Hello, depends on what do you need (large crystals or small ones)
G.PattonHello, what is the best way to obtain large crystals, if the crystallization time would be a maximum of 7 days?
 
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G.Patton

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Hello, what is the best way to obtain large crystals, if the crystallization time would be a maximum of 7 days?
SonicNLHi. You have to carry out recrystallization and cool a salt solution down as slower as possible without shaking a crystallization dish.
 

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Hi. You have to carry out recrystallization and cool a salt solution down as slower as possible without shaking a crystallization dish.
G.PattonThanks. What method would you prefer to use in this case? IPA/water 50/50 good at +- 18 C?
 

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ChemDamn

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An interesting cabinet
subzero013hermetic cabinet, the seams are smeared with sealant, extractor hood, dehumidifier. allows you to maintain a constant temperature and humidity for the isothermal crystallization method
 
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subzero013

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hermetic cabinet, the seams are smeared with sealant, extractor hood, dehumidifier. allows you to maintain a constant temperature and humidity for the isothermal crystallization method
ChemDamnI read his article about this particular cabinet. it's a pity that he stopped publishing his articles, the most interesting ones and did not come out.
 
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AsaLT

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here is my result with this method. The method is quite simple and fast. but NaCl or CaCl is not needed here at all. all you need is water and 4-mmc. bring water to a boil and dissolve 4-mmc (1g per 1ml) in it. continue to boil until the surface of the solution is covered with a film. then pour the solution into a glass container with a layer of ~ 5 cm and leave it completely at rest for 10 hours. I did this at a room temperature of + 8C. after 10 hours the crystals are ready
ChemDamnHi, I have a few questions about your method:
1) What kind of water did you use in this method (distilled, flowing, minimal, bottled),
2) At what temperature the solution was boiled
3) At what point the powder is added, all at once or in certain portions
4) During boiling, stir the solution or leave it alone
5) After boiling, the solution was poured into a crystallization container?
 

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Well-cleaned powder, low dissolving temp and this is what it looks like after standing motionless at room temperature for 18h
 

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Didi

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Wodka 40% pure and Vitamin C pure and u have maximal pure crystal later wash with acetone and this all
 

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I am not saying that I have to be completely right.

I saw a post here on the forum by another user who mentioned an ascorbic acid supplement.

I put down some 4MMC powder from a batch and added the said vitamin C to its crystallisation.

The final crystal with vitamin C, at least in my case, made the crystal very brittle, plus it just got greasy after a few days outdoors.

Who knows, maybe I made a mistake. No less from my side this is how it looked. Regards
 

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I confirm your words. The addition of vitamin C leads to loss of color during storage of the product.
 

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@G.Pattong As promised, I crystallized the way discussed here and here is the result.

I've washed the product again and i'm going to repeat the crystallization process.
 

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$!$

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@G.Pattong As promised, I crystallized the way discussed here and here is the result.

I've washed the product again and i'm going to repeat the crystallization process.
SonicNLbecause your powder was dirty and u get it i made also this time form dirty im shure i get the same but i was mix water with acetone but water i was use morw like acetone
 
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