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It should be ok because you crashed ot out in acetone. More acid just makes more impurities.
Did you get big crystals from pouring the hot acidified freebase into cold acetone?
Did you get big crystals from pouring the hot acidified freebase into cold acetone?
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It should be ok because you crashed ot out in acetone. More acid just makes more impurities.
Did you get big crystals from pouring the hot acidified freebase into cold acetone?
Thanks.
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btcboss2022I adjusted the freebase to ph3 and heated it up, I added a little cold acetone and these crystals were born... I added 4 times more acetone and put it in the freezer
kharpa177I Guess thats not the my way then.If you are asking me about issues with a different process you should explain the previous steps.
btcboss2022
I made this synthesis only at the end that I crystallized in the way you said
btcboss2022.
btcboss2022
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- By kharpa177
What step is this one?
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I adjusted the freebase to ph3 and heated it up, I added a little cold acetone and these crystals were born... I added 4 times more acetone and put it in the freezer
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I Guess thats not the my way then.If you are asking me about issues with a different process you should explain the previous steps.
I made this synthesis only at the end that I crystallized in the way you said
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I Guess thats not the my way then.If you are asking me about issues with a different process you should explain the previous steps.
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I Guess thats not the my way then.If you are asking me about issues with a different process you should explain the previous steps.